Preparation technology of polygonatum polysaccharide peptide
A polysaccharide polysaccharide and a preparation process technology are applied in the field of preparation technology of polysaccharide polysaccharide peptides, which can solve problems such as research difficulties, and achieve the effects of high purity, low production cost and good product quality.
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[0020] 1) Preparation:
[0021] Wash the Rhizome of Rhizoma Polygonatum, dry it at 80°C to constant weight, and crush it through a 60-mesh sieve. Weigh a certain amount of Rhizoma Polygonati dry powder in the Erlenmeyer flask of the reflux extractor, then add water with 10 times the weight of Rhizoma Rhizoma Polygonatum as the extraction solvent.
[0022] 2) Extraction and preliminary purification:
[0023] Move the Erlenmeyer flask to an electric furnace and heat it to 80°C, then move it to a constant temperature water bath, keep the extraction temperature at 80°C for hot water leaching for 2 hours, and extract twice; combine the extracts, concentrate under reduced pressure to 1 / 2 the total volume, add h 2 o 2 Make H 2 o 2 The final concentration is 1% (mass percentage), 60 ° C constant temperature decolorization for 30 minutes, then add the equivalent of 1 / 2 H 2 o 2 Amount (molar amount) of Na 2 SO 3 to remove hydrogen peroxide; then add an equal volume of 6% trichl...
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