Unlock instant, AI-driven research and patent intelligence for your innovation.

Method for preparing stable oil-in-water emulsion with high oil phase content, emulsion prepared by method and application of emulsion

A technology of oil-in-water emulsion and oil phase, which is applied in the field of oil-in-water emulsion, personal care and cosmetic products. a week and so on

Inactive Publication Date: 2013-09-04
TH GOLDSCHMIDT AG
View PDF4 Cites 8 Cited by
  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In most embodiments of CN1175805C, only enumerate the situation that oil phase is 20wt%; The oil phase content prepared in embodiment 18 is the emulsion of 80% only intermediate product; , but its stability data is only one week, which cannot meet the needs of actual production and use
That is to say, adopting the formula of this invention, it is actually difficult to obtain a high oil phase content emulsion that meets the actual production needs, especially it is difficult to obtain a stable high oil phase content oil-in-water emulsion

Method used

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
View more

Image

Smart Image Click on the blue labels to locate them in the text.
Viewing Examples
Smart Image
  • Method for preparing stable oil-in-water emulsion with high oil phase content, emulsion prepared by method and application of emulsion
  • Method for preparing stable oil-in-water emulsion with high oil phase content, emulsion prepared by method and application of emulsion
  • Method for preparing stable oil-in-water emulsion with high oil phase content, emulsion prepared by method and application of emulsion

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1-3

[0068] The formulations of Examples 1-3 are shown in Table 1 below.

[0069] Table 1

[0070]

[0071] Product 1 was prepared according to the following steps:

[0072] (i) 3wt.% glycerin, 0.1wt.% xanthan gum, 1wt.% emulsifier Add Care450 and 0.1wt.% preservative chloroacetamide in sequence to 10.8wt.% water, mix, heat to 80°C, and stir evenly to obtain phase B;

[0073] (ii) under the stirring speed of 800rpm will be by 45wt.% SOFT OP and 40wt.% The liquid oil phase A composed of SOFT DEC is added to the phase B obtained in step (a) within 5 minutes (that is, the speed of adding 19wt.% oil phase per minute), and the whole system remains uniform throughout the addition process emulsified state; and

[0074] (iii) After the oil phase A is added, increase the stirring speed to 10,000 rpm for homogenization (homogenization), and obtain an oil-in-water emulsified product 1 with a high content of the oil phase, totaling 200 g.

[0075] In this example, the step (ii) has...

Embodiment 4

[0081] The formulation of the oil-in-water emulsion of Example 4 is shown in Table 2 below.

[0082] Table 2

[0083]

[0084]

[0085]In a manner similar to the preparation of Product 1 in Example 1, an oil-in-water emulsion with the formulation of Table 2 above was prepared by adding 85 wt.% of the oil phase A within 15 minutes (i.e., adding 5.6 wt.% of the oil phase A per minute) Speed) stirring and adding to phase B, and finally product 4 was obtained, with a total amount of 1000g. The emulsion obtained in this example has a milky white creamy appearance and good stability: Product 4 was subjected to room temperature stability test, heat resistance test and freeze-thaw test respectively. The room temperature stability test means that the sample is stored at room temperature between 20-25 °C for three months, the heat resistance test means that the sample is stored at 45 °C for three months, and the freeze-thaw test means that the sample is stored at -15 °C / room temp...

Embodiment 5

[0087] The formula of the oil-in-water emulsion of embodiment 5 is as shown in table 3 below:

[0088] table 3

[0089]

[0090] In a manner similar to the preparation of Product 1 in Example 1, an oil-in-water emulsion with the formulation of Table 3 above was prepared by adding 55 wt.% of the oil phase A within 5 minutes (i.e., the rate of adding 11 wt.% of the oil phase per minute ) was stirred and added to phase B, and finally product 5 was obtained, with a total amount of 2000g. The emulsion obtained in this example has a milky white creamy appearance; product 5 was subjected to room temperature stability test, heat resistance test and freeze-thaw test respectively. The room temperature stability test means that the sample is stored at room temperature between 20-25 °C for three months, the heat resistance test means that the sample is stored at 45 °C for three months, and the freeze-thaw test means that the sample is stored at -15 °C / room temperature Three hot and c...

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

PUM

PropertyMeasurementUnit
Freezing temperatureaaaaaaaaaa
Login to View More

Abstract

The invention relates to a method for preparing a stable oil-in-water emulsion with high oil phase content, the oil-in-water emulsion prepared by the method and application of the emulsion. The emulsion prepared by the method has high oil phase content, and can be widely applied to individual nursing and cosmetic products. The oil-in-water emulsion has milk-white downy appearance or can be changed to transparent jelly appearance as required, can rapidly release nourishing grease while being smeared, achieves multifunctional functions of removing color cosmetics, massaging, keeping humidity and the like, and can also substitute for baby oil.

Description

[0001] This application is a divisional application of the Chinese invention patent application 200810178780.3 filed on December 1, 2008, with the title of the invention "Method for preparing stable oil-in-water emulsion with high oil phase content, the emulsion prepared therefrom and its application" . technical field [0002] The present invention relates to a method for preparing a stable oil-in-water emulsion with a high oil phase content, the oil-in-water emulsion prepared thereby and its application, and the emulsion can be widely used in personal care and cosmetic products. Background technique [0003] Pure oil or pure oil composition products have existed in the field of personal care and cosmetics for a long time, but they have many disadvantages, such as high permeability, high packaging requirements, and inconvenient use of liquid products. Although directly thickening the oil agent can overcome the above shortcomings, it will bring new problems, such as difficul...

Claims

the structure of the environmentally friendly knitted fabric provided by the present invention; figure 2 Flow chart of the yarn wrapping machine for environmentally friendly knitted fabrics and storage devices; image 3 Is the parameter map of the yarn covering machine
Login to View More

Application Information

Patent Timeline
no application Login to View More
IPC IPC(8): B01F3/08A61K8/06A61Q1/14A61Q19/00A61Q17/04
Inventor 张海州戴静亚邹佳丽高志恒
Owner TH GOLDSCHMIDT AG