Dental prosthetic material and preparation method thereof
A restoration material and a dental technology, applied in the field of dental restoration materials and their preparation, can solve the problems of partial reduction of natural enamel, enlargement of caries, mechanical properties failing to reach the strength of enamel, and the like, achieving mild conditions, cheap raw materials, and simple process Effect
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Embodiment 1
[0034] Embodiment 1, preparation dental restorative material
[0035] Take isolated human molars or wisdom teeth, use the side of the saw blade of a low-speed diamond cutter to gently grind the enamel surface, and cut off the enamel part. Treat the above enamel with 85% phosphoric acid aqueous solution by mass for 30 seconds, rinse off the residual acid solution with deionized water, and set aside.
[0036] Weigh 236.00g Ca(NO 3 ) 2 4H 2 O was added about 800mL deionized water, and the 1000mL volumetric flask was constant to obtain Ca(NO 3 ) 2 solution. Weigh 0.30g agarose (Agarose), add 8mL Ca(NO 3 ) 2 solution, and 7.2mL of water was added, stirred with a glass rod and heated to boiling to obtain Agarose-Ca solution, the pH value of which was 7.0, wherein the ratio of agarose to calcium nitrate was 1g: 0.027mol, the mass percentage of agarose The content is 1.97%, and the molar concentration of calcium nitrate is 0.526mol / L.
[0037] Weigh 136.00g KH 2 PO 4 and 31...
Embodiment 2
[0048] Embodiment 2, preparation dental restorative material
[0049] Weigh 236.00g Ca(NO 3 ) 2 4H 2 O was added about 800mL deionized water, and the 1000mL volumetric flask was constant to obtain Ca(NO 3 ) 2 solution. Weigh 0.20g agarose (Agarose), add 6mL Ca(NO 3 ) 2 solution, and add 10.4mL of water, stir with a glass rod and heat to boiling to obtain Agarose-Ca solution, its pH value is 7.0, wherein the ratio of agarose to calcium nitrate is 1g:0.03mol, the mass percentage of agarose The content is 1.22%, and the molar concentration of calcium nitrate is 0.366mol / L.
[0050] Weigh 136.00g KH 2 PO 4 and 31.33g KF 2H 2 0, 1000mL volumetric flask is constant volume, obtains phosphate ion and fluoride ion solution, and wherein, the molar concentration of phosphate ion is 1.0mol / L, and the molar concentration of fluoride ion is 0.33mol / L.
[0051] Measure 3.6 mL of phosphate ion and fluoride ion solution, add hot Agarose-Ca solution to obtain a mixed solution, place ...
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