The invention belongs to the technical field of medical
prosthesis materials, and particularly relates to a medical
implant material based on hydrothermal method
surface modification and a preparation method and application thereof.The preparation method comprises the steps that S1,
zirconium oxide preform surface pretreatment is conducted, specifically, firstly, a
zirconium oxide preform is sintered, and then
surface grinding,
polishing and cleaning are conducted; s2, preparation of the
zirconium oxide surface micro-nano structure: putting the
zirconium oxide preform into a high-pressure reaction kettle, adding a
phosphoric acid solution containing
metal ions, putting the high-pressure reaction kettle into a
drying oven, reacting for 20-28 hours at 150-170 DEG C, taking out the
zirconium oxide implant material after the reaction is completed, cleaning and
drying to obtain the medical
implant material subjected to
surface modification based on the hydrothermal method, and
drying to obtain the
zirconium oxide surface micro-nano structure. According to the invention, a micro-nano structure doped with different
metal ions is successfully constructed on the surface of the ZrO2 preform by adopting a
phosphoric acid hydrothermal method, the surface of each
doping group shows different micro-nano morphological characteristics, the
metal ions on the surface of the material can be slowly released, and excellent surface biological performance is shown.