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463 results about "Material analysis" patented technology

Method for direct recovery and restoration of lithium ion battery positive electrode material

The invention discloses a method for direct recovery and restoration of a lithium ion battery positive electrode material, and belongs to the field of resource recycling. According to the method, waste positive electrode pieces of lithium cobaltate or lithium nickel manganese cobalt multi-element layered oxide or a positive electrode piece leftover material and defective products are used as a positive electrode material; the materials are classified according to the type of binder by component analysis, the binder is directly damaged, cleaning and separation of the positive electrode material and a current collector are realized; by use of a heavy liquid separation principle, the positive electrode and a conductive agent are separated; the positive electrode failure mechanism is studied by use of SEM (scanning electron microscope), XRD (X-ray diffraction), STEM (scanning transmission electron microscope), XPS (X-ray photoelectron spectroscopy) and other analysis means; chemical components of the positive electrode material with the layered structure not damaged can be repaired by high temperature roasting, the layered structure of the positive electrode material with disordered and defective crystal lattice can be repaired by dissolving with a hydrothermal reaction and then precipitation, and the positive electrode material with good charge discharge performances can be again obtained. The method avoids the dissolving leaching process, reduces waste liquid generation, and simplifies the technological process.
Owner:INST OF PROCESS ENG CHINESE ACAD OF SCI

Bidirectional test device and test method for single-shaft material test machine

The invention provides a bidirectional test device and a test method for a single-shaft material test machine. The bidirectional test device comprises a machine frame, two slide blocks and a measuring device, wherein the machine frame comprises two side frames in opposite arrangement; the two ends of the opposite sides of the two side frames are provided with relatively projected triangular end wings; the two slide blocks are movably fixed between the two side frames in a way of being clamped by the end wings arranged at the two ends of the two side frames; a space defined by the machine frame and the slide blocks is a test specimen installing space; the measuring device comprises measuring springs and displacement sensors; each measuring spring is arranged at one end, in contact with the slide block and the test specimen, of each side frame; the displacement sensors are used for detecting the displacement of the measuring springs. The bidirectional test device has the function of realizing bidirectional stretching and bidirectional compression on a single-axis material test machine; the loading synchronization problem is solved; meanwhile, the bidirectional test device can accurately measure the force and the displacement of the test specimen during the stretching and compression loading, so that an important stress-stress relationship curve during the material analysis can be given.
Owner:INST OF MECHANICS - CHINESE ACAD OF SCI

Laser-induced breakdown spectrum in-situ analyzer

The invention provides a laser-induced breakdown spectrum in-situ analyzer, belonging to the technical field of material analysis and characterization. The laser-induced breakdown spectrum in-situ analyzer comprises an excitation source system, a laser beam shaping system, a beam splitting system, a high-speed signal collecting system, a signal analyzing system, a sample chamber vacuum system, a continuous excitation synchronous scanning and positioning system and a sample surface imaging system. The laser beam emitted by the laser source is processed by a laser beam shaping system and is subsequently focused on the surface of an analyzed sample that can move in a three-dimensional way. The sample chamber vacuum system provides a closed environment for the analyzed sample so as to fill inthe protective gas. The beam splitting system and the signal colleting system are connected with each other by a photomultiplier; and the plasma spectrum generated on the surface of the sample is converted into an electric signal by the photomultiplier through the optical signal generated by the beam splitting system. The data processing system processes and calculates the photoelectric signal generated by the data processing system and outputs the results such as content of each element, in-situ statistics distribution and the like in the sample. Compared with the prior art, the laser-induced breakdown spectrum in-situ analyzer has the advantages of increasing the functions and extending the sample scope.
Owner:NCS TESTING TECH

Microscopic Raman imaging spectrum rapid detection apparatus and method thereof

The invention discloses a microscopic Raman imaging spectrum rapid detection apparatus and a method thereof, which belong to the technical field of optical microscopic imaging and spectral measurement. The microscopic Raman imaging spectrum rapid detection apparatus comprises a light source, a multifunctional sample room, a composite optical system, an image acquisition system, a data fusion processing system, a Raman spectrum detection system, and a computer control and display system. According to white light or laser emitted by the light source, sample in-situ observation and microscopic Raman imaging spectrum real-time on-line detection are respectively realized, the data fusion processing system performs real-time analysis processing on images and spectrum information, and images andspectrum information are displayed and output in the computer control and display system. The microscopic Raman imaging spectrum rapid detection apparatus has the characteristics of compact structure,high spatial resolution, convenient usage, and stable performance, can be used in the fields of water quality detection, material analysis, petrochemical engineering, environment monitoring, and industrial precision detection, is convenient for field on-site investigation experiment and on-line test real-time analysis, and has a wide application prospect.
Owner:CHONGQING INST OF GREEN & INTELLIGENT TECH CHINESE ACADEMY OF SCI

LA-ICPMS (laser ablation inductively coupled plasma mass spectrometry) based original position statistic distribution analysis system

InactiveCN102375022AHigh sensitivityPreparing sample for investigationMaterial analysis by electric/magnetic meansLaser ablation inductively coupled plasma mass spectrometryMetallic materials
The invention discloses an LA-ICPMS (laser ablation inductively coupled plasma mass spectrometry) based original position statistic distribution analysis system and belongs to the technical field of material analysis characterization. The system disclosed by the invention comprises a laser ablation sample-injection system, an ICP (inductively coupled plasma) ion source system, an interface system, an ion transmission system, a mass spectrum detection system, a sample moving/positioning system and a signal processing system, wherein the sample moving/positioning system is used for continuously activating synchronous scanning, and the signal processing system is used for carrying out mathematical resolution on acquired mass spectrum signals. By using the system disclosed by the invention, based on the continuously-activated synchronous scanning moving/positioning of samples and the laser ablation inductively coupled plasma mass spectrometry (LA-ICPMS), an original position statistic distribution analysis on chemical compositions and states thereof in large-scale ranges of uneven surfaces of metallic and non-metallic materials can be realized. The system disclosed by the invention has the advantages that the system can be used for metal samples and appropriate for non-metallic samples as well; the content and distribution of an element (as low as 0.1 mu g/g) can be analyzed; compared with an original position analyzer for metals, the sensitivity is increased by three orders of magnitude; and the system is suitable for samples with regular and even surfaces and samples with irregular or special-shaped surfaces.
Owner:NCS TESTING TECH
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