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Improved polymerization reactor

A polymerization reactor, import and export technology, applied in polymerization reaction. , In the field of polymerization reactors, it can solve the problems of increased acetaldehyde content of impurities, increased impurities, and consumption of cooling water, etc., and achieve the effects of improved catalyst activity, increased production capacity, and improved production efficiency

Inactive Publication Date: 2013-09-25
NANJING HAOYANG CHEM EQUIP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In the traditional polymerization reactor, the heat transfer effect of the reactor is poor, and the content of impurity acetaldehyde in the reaction product increases, so that the reaction polymer increases, the heat transfer effect is worse, and the impurity is further increased, thus forming a vicious circle
[0003] In addition, the polymerization reaction is an exothermic reaction, and the heat released by the reaction is only used to preheat the circulating air, and most of the remaining heat is taken away by the heat transfer oil cooler and the mixed cooling system, which consumes a lot of cooling water and causes precious natural waste

Method used

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  • Improved polymerization reactor

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Embodiment

[0015] Example: The polymerization reactor in this embodiment is in the form of a shell-side cylinder and a tube-side heat exchange tube, as shown in the attached figure 1 As shown, the main structure includes an upper head 1, a shell-side cylinder 8, a conical head 11, an upper tube sheet 3, a lower tube sheet 14, and a heat exchange tube 15. The main improvement is that a The upper annular flow channel 4 and the lower annular flow channel 10, and small holes of different diameters are opened in the corresponding positions of the shell-side cylinder 8; three baffle support plates are arranged in the shell-side cylinder 8 along the direction of the heat exchange tubes, and the middle baffle A hole of φ250mm is set in the middle of the support plate 6, and 120 small holes of φ10mm are respectively arranged on the upper baffle support plate 5 and the lower baffle support plate 9.

[0016] In the embodiment, the upper head 1 is an EHA standard elliptical head, the upper head 1 ...

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Abstract

The invention belongs to the technical field of chemical equipment and relates to a polymerization reactor, particularly to a reactor composed of a shell-side cylindrical shell and a tube-side heat exchange tube, especially to a reactor for polymerization in PAVC production. The reactor provided by the invention comprises a structure composed of the shell-side cylindrical shell and the tube-side heat exchange tube and is characterized in that ring runners are arranged along the circumference of the shell-side cylindrical shell at conduction oil inlet and outlet of the shell-side cylindrical shell; the shell-side cylindrical shell inside the ring runners is provided with several small holes for flowing of conduction oil; three baffling shoe plates are arranged along the direction of the heat exchange tube inside the shell-side cylindrical shell; a big hole is disposed in the center of the middle baffling shoe plate; and the upper and lower baffling shoe plates are provided with several small holes. According to the invention, conduction oil uniformly enters the shell side so as to make the shell-side temperature to be controlled and make the temperature rise and decrease uniformly. Production efficiency is raised while a catalyst is used to the maximum. Through improvement of the equipment structure, temperature difference of the conduction oil inlet and outlet is well controlled, temperature variation is controlled within 1%, activity of the catalyst is raised by 10%, and production capacity is enhanced by more than 30%.

Description

technical field [0001] The invention belongs to the technical field of chemical equipment, and relates to a polymerization reactor, in particular to a reactor composed of a shell-side cylinder body and a tube-side heat exchange tube, especially for polymerization reaction in PAVC production. Background technique [0002] In the traditional polymerization reactor, the heat transfer effect of the reactor is poor, and the content of impurity acetaldehyde in the reaction product increases, so that the reaction polymer increases, the heat transfer effect is worse, and the impurity is further increased, thus forming a vicious circle . [0003] In addition, the polymerization reaction is an exothermic reaction, and the heat released by the reaction is only used to preheat the circulating air, and most of the remaining heat is taken away by the heat transfer oil cooler and the mixed cooling system, which consumes a lot of cooling water and causes precious natural waste . Contents...

Claims

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Application Information

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IPC IPC(8): B01J19/00C08F118/08C08F8/00C08F2/01
Inventor 高驰顾天平高昊杨平化
Owner NANJING HAOYANG CHEM EQUIP
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