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Improved polymerization reactor

A polymerization reactor, import and export technology, applied in chemical instruments and methods, chemical/physical/physical chemical processes, chemical/physical processes, etc., can solve the problems of increased impurity acetaldehyde content, consumption of cooling water, and increased impurities. , to achieve the effect of improved catalyst activity, uniform temperature rise and fall, and improved production capacity

Inactive Publication Date: 2014-02-12
NANJING HAOYANG CHEM EQUIP
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] In the traditional polymerization reactor, the heat transfer effect of the reactor is poor, and the content of impurity acetaldehyde in the reaction product increases, so that the reaction polymer increases, the heat transfer effect is worse, and the impurity is further increased, thus forming a vicious circle
[0003] In addition, the polymerization reaction is an exothermic reaction, and the heat released by the reaction is only used to preheat the circulating air, and most of the remaining heat is taken away by the heat transfer oil cooler and the mixed cooling system, which consumes a lot of cooling water and causes precious natural waste

Method used

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  • Improved polymerization reactor

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Embodiment

[0015] Example: The polymerization reactor in this embodiment is in the form of a shell-side cylinder and a tube-side heat exchange tube, as shown in the attached figure 1 As shown, the main structure includes an upper head 1, a shell-side cylinder 8, a conical head 11, an upper tube sheet 3, a lower tube sheet 14, and a heat exchange tube 15. The main improvement is that a The upper annular flow channel 4 and the lower annular flow channel 10, and small holes of different diameters are opened in the corresponding positions of the shell-side cylinder 8; three baffle support plates are arranged in the shell-side cylinder 8 along the direction of the heat exchange tubes, and the middle baffle A hole of φ250mm is set in the middle of the support plate 6, and 120 small holes of φ10mm are respectively arranged on the upper baffle support plate 5 and the lower baffle support plate 9.

[0016] In the embodiment, the upper head 1 is an EHA standard elliptical head, the upper head 1 ...

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Abstract

The invention belongs to the technical field of chemical equipment, relates to a polymerization reactor, particularly relates to a reactor consisting of a shell pass barrel and a shell pass heat exchange tube, and is especially applied to a polymerization reaction in PAVC production. The improved polymerization reactor comprises a shell pass barrel and a shell pass heat exchange tube structure; the improved polymerization reactor is characterized in that a heat-conducting oil exit of the shell pass barrel is provided with an annular runner along the circumference of the shell pass barrel; the shell pass barrel in the annular runner is provided with multiple small holes for heat-conducting oil flowing; three baffle support plates are arranged in the shell pass barrel along the direction of a heat exchange tube, the middle of the middle baffle support plate is provided with a large hole, and the uppermost and bottommost baffle support plates are provided with multiple small holes. According to the invention, heat-conducting oil uniformly enters a shell pass, so that the temperature of the shell pass is controlled, and the temperature increasing and reducing is uniform; a catalyst is maximumly used while the production efficiency is improved. Through the improvement of an equipment structure, the temperature difference of the heat-conducting oil exit is controlled well, so that the temperature change is controlled within 1%, the activity of the catalyst is increased by 10%, and the production capacity is increased by more than 30%.

Description

technical field [0001] The invention belongs to the technical field of chemical equipment, and relates to a polymerization reactor, in particular to a reactor composed of a shell-side cylinder body and a tube-side heat exchange tube, especially for polymerization reaction in PAVC production. Background technique [0002] In the traditional polymerization reactor, the heat transfer effect of the reactor is poor, and the content of impurity acetaldehyde in the reaction product increases, so that the reaction polymer increases, the heat transfer effect is worse, and the impurity is further increased, thus forming a vicious circle . [0003] In addition, the polymerization reaction is an exothermic reaction, and the heat released by the reaction is only used to preheat the circulating air, and most of the remaining heat is taken away by the heat transfer oil cooler and the mixed cooling system, which consumes a lot of cooling water and causes precious natural waste . Contents...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J19/00C08F118/08C08F2/01
Inventor 高驰顾天平高昊杨平化
Owner NANJING HAOYANG CHEM EQUIP
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