Device and method for quickly measuring carbon dioxide flux of soil

A technology for rapid determination of carbon dioxide, used in soil material testing, material inspection products, etc.

Inactive Publication Date: 2014-03-12
NANJING UNIV OF INFORMATION SCI & TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

In the past, the observation methods and equipment of soil CO2 flux were mainly aimed at the observation of field soil CO2 emissions. The observation instruments mainly include static box-gas chromatography, portable soil respiration However, there are some problems in these research methods: when the observation site is in the field, the observed soil CO2 flux includes root respiration and soil heterotrophic respiration, and cannot focus on soil CO2The influence factors and mechanism of emissions are studied; when the soil samples are collected back to the laboratory to analyze the CO2 flux, if the design of the gas extraction port is unreasonable, the pressure in the closed container will be too high, and then Affect the gas flux measurement effect, the reliability of the experimental results is also greatly reduced, and the expected experimental purpose cannot be achieved
Therefore, it is necessary to use a new method to solve the problem of inaccurate measurement of soil CO2 flux, and provide the necessary experimental equipment for the research of farmland soil carbon cycle.

Method used

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  • Device and method for quickly measuring carbon dioxide flux of soil
  • Device and method for quickly measuring carbon dioxide flux of soil
  • Device and method for quickly measuring carbon dioxide flux of soil

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0027] Example 1 Determination of soil CO 2 Flux devices and methods

[0028] A method for measuring soil CO 2 Flux devices and methods, see figure 1 As shown, the device includes a glass bottle 1 with a bottle cap 2, an air guide port 3, an air guide tube 4, CO 2 Analyzer 5, cap screwed onto glass vial, connected to CO via gas port 3 and gas line 4 2 On analyzer 5, the glass bottle has a capacity of 825 ml and an outer diameter of 8 cm. The matching bottle cap of the glass bottle is made of stainless steel, and the outer diameter of the bottle cap is 8 cm. Two drilling holes 6 are arranged at a distance of 3 cm from the two edges along the diameter of the bottle cap, and each drilling hole has a diameter of 3 mm. Insert a threaded screw 7 with a length of 29 mm into each drill hole, the threaded screw is made of copper, and the inner diameter of the threaded screw is 2 mm. Use a hexagonal steel washer 8 to seal the contact surface between the threaded screw and the inne...

Embodiment 2

[0031] Example 2: Effects of different exogenous nitrogen additions on soil CO 2 Effect of flux

[0032] The experiment was divided into three stages: soil addition and pre-incubation, treatment and analytical determination.

[0033] Soil addition and pre-cultivation: Weigh 60 g of soil sieved with a 2 mm soil sieve, spread it into a glass bottle, add water with a graduated cylinder, adjust the water content to 25%, air-dry the soil and water to a total of 80 grams, and cultivate Pre-cultivate for 10 days in a box at 20°C. Add water regularly every day to keep the water content at 25%.

[0034] Treatment: The exogenous nitrogen used in the experiment was ammonium nitrate, and 17 gradients of ammonium nitrate were set: 0.0000 g (CK), 0.0001 g, 0.0003 g, 0.0006 g, 0.0010 g, 0.0015 g, 0.0021 g, 0.0028 g, 0.0036 g, 0.0045 g, 0.0055 g, 0.0066 g, 0.0078 g, 0.0091 g, 0.0200 g, 0.0500 g, 0.100 g. Add water regularly every day to keep the water content at 25%.

[0035] Ana...

Embodiment 3

[0038] Example 3: Effect of different straw additions on soil CO 2 Effect of flux

[0039] Adopt the measurement soil CO of embodiment 1 2Flux method for soil CO 2 Flux is measured, open the CO 2 The analyzer is preheated, and the stainless steel bottle cap with the gas collection interface is connected to the CO through the gas collection port and the gas guide tube. 2 on the analyzer. Take out the glass bottle from the incubator, screw the stainless steel bottle cap onto the glass bottle to form a loop closed path, and start the measurement.

[0040] This example includes three stages of soil addition and pre-cultivation, treatment, analysis and determination. Wherein the pre-cultivation step is the same as that in Example 1.

[0041] Treatment: Dry the wheat straw in advance, grind it into powder, set 15 straw addition levels, namely: 0.0000 g (CK), 0.001g, 0.003g, 0.050g, 0.070g, 0.090g, 0.110g, 0.130g, 0.150 g, 0.170g, 0.190g, 0.210g, 0.230g, 0.250g, 0.270g, accura...

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Abstract

The invention discloses a device and a method for quickly measuring the carbon dioxide flux of soil. The device comprises a glass bottle, a bottle cover with gas collection ports, gas guide pipes and a CO2 analyzer, wherein the bottle cover is screwed on the glass bottle and is connected to the CO2 analyzer through the gas collection ports and the gas guide pipes; drilled holes are formed in the bottle cover; threaded screws are inserted into the drilled holes, and gaskets are used for sealing contact surfaces of the threaded screws and the bottle cover; a circular protruded part is arranged on the part, which is exposed out of the bottle cover, above each threaded screw; inwards sunken grooves are formed in the protruded parts. According to the device and the method which are disclosed by the invention, a dynamic circulating process in a closed pipeline is formed, so that the phenomenon that gas cannot flow is avoided, and the accuracy of a measured result is improved. The measurement time is short, and the shortest measurement time can be set to be within 1-3 minutes; the next sample can be immediately measured as soon as a soil sample is measured, so that the quick measurement of batches of soil samples can be realized.

Description

Technical field [0001] The invention is the field of ecological and meteorological environmental regulation, and it involves a device and method that quickly determines the flux of the soil carbon dioxide. Background technique [0002] Soil CO 2 The flux is an important process in the carbon cycle. 2 The estimation value of the carbon released to the atmosphere is about 50 ~ 120 pg (1 pg = 1 × 10 15 g), the value is second only to the estimated values of the global general primary productivity (GPP).At present, people have relatively many research on the "ground" process in the ecosystem, and the research on the "underground" process is not thorough, and soil respiration has an important impact on ecosystem carbon balance. 2 The process and its influence factor are extremely critical to understanding the land carbon cycle. [0003] Due to soil CO 2 The important role of flux in the carbon cycle, domestic and foreign scientists have already on soil CO 2 Some research methods, proc...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N33/24
Inventor 陈书涛胡正华刘燕高慧王圆媛汪萌李宏娜
Owner NANJING UNIV OF INFORMATION SCI & TECH
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