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Zinc hydrogen citrate ascorbate and its preparation method and application

A technology of zinc ascorbate and ascorbic acid, applied in the field of biochemical medicine, medicine and food, can solve the problems such as use restriction, difficult absorption by humans and animals, and achieve the effects of reducing costs, being beneficial to human body absorption, and improving market prospects.

Inactive Publication Date: 2016-07-13
李玉成
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0002] Zinc citrate in the biochemical, pharmaceutical and food markets at home and abroad today, English name: ZincCitrate, molecular formula: Zn 3 (C 6 h 5 o 7 ) 2 2H 2 O, with a purity of 98.0-100.5% or more (medicine and food grade), is a white crystalline powder. It is a smart food additive for zinc supplementation and a medicine for treating loss of appetite and dysplasia. However, because it is insoluble in water, it is difficult for humans and animals to absorb. restrict its use

Method used

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  • Zinc hydrogen citrate ascorbate and its preparation method and application

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Embodiment 1

[0028] The preparation method flowchart of hydrogen citrate zinc ascorbate is as figure 1 shown.

[0029] The preparation method of the present embodiment hydrogen citrate ascorbate zinc, comprises the following steps:

[0030] (1) Weigh 630.42g of citric acid monohydrate, 176.13g of ascorbic acid, 325.52g of zinc oxide and a certain amount of water, and put the raw materials into the reaction kettle together;

[0031] (2) Start the chemical reaction for half an hour, the chemical reaction formula is:

[0032] 3(C 6 h 8 o 7 )·H 2 O+C 6 h 8 o 6 +4ZnO=Zn 4 h 2 (C 6 h 7 o 6 )(C 6 h 5 o 7 ) 3 4H 2 O↓+3H 2 O, the reaction condition is normal temperature;

[0033] (3) Shut down for half an hour, add ethanol to make the chemical reaction mature, and precipitate zinc hydrogen citrate ascorbate crystals;

[0034] (4) Start the machine for half an hour, then filter and wash the materials in the reactor after the reaction, and release hydrogen citrate and zinc ascorb...

Embodiment 2

[0037] The preparation method flowchart of hydrogen citrate zinc ascorbate is as figure 1 shown.

[0038] The preparation method of the present embodiment hydrogen citrate ascorbate zinc, comprises the following steps:

[0039] (1) Weigh 1260.84g of citric acid monohydrate, 352.26g of ascorbic acid, 651.04g of zinc oxide and a certain amount of water, and put the raw materials into the reaction kettle together;

[0040] (2) Start the chemical reaction for half an hour, the chemical reaction formula is:

[0041] 3(C 6 h 8 o 7 )·H 2 O+C 6 h 8 o 6 +4ZnO=Zn 4 h 2 (C 6 h 7 o 6 )(C 6 h 5 o 7 ) 3 4H 2 O↓+3H 2 O, the reaction condition is normal temperature;

[0042] (3) Shut down for half an hour, add ethanol to make the chemical reaction mature, and precipitate zinc hydrogen citrate ascorbate crystals;

[0043] (4) Start the machine for half an hour, then filter and wash the materials in the reactor after the reaction, and release hydrogen citrate and zinc ascor...

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Abstract

The invention relates to a new substance, namely zinc ascorbate hydrogen citrate, as well as a preparation method and an application thereof. The preparation method of the zinc ascorbate hydrogen citrate is characterized by comprising the following steps: (1) weighing raw materials, namely citric acid monohydrate, ascorbic acid, zinc oxide and water, and putting into a reaction kettle, wherein the weight ratio of the substances, namely the citric acid monohydrate, the ascorbic acid and the zinc oxide is 3: 1: 4; (2) starting a machine for performing chemical reaction for half an hour; (3) stopping the machine for half an hour, adding ethanol and enabling the chemical reaction to be mature; and (4) starting the machine for half an hour, and releasing the zinc ascorbate hydrogen citrate. The zinc ascorbate hydrogen citrate prepared by the preparation method provided by the invention can be dissolved in water, be conductive to absorption by people and animals, and be used as a zinc supplement Vc anti-oxidation preservative, a zinc supplement Vc food additive or medicines for treating bad appetite, dysplasia, stomach diseases, bronchitis, asthma, pneumonia, hepatitis, liver cancer and hypertension.

Description

technical field [0001] The invention relates to the field of biochemical industry, medicine and food, in particular to zinc hydrogen citrate ascorbate and its preparation method and application. Background technique [0002] Zinc citrate in the biochemical, pharmaceutical and food markets at home and abroad today, English name: ZincCitrate, molecular formula: Zn 3 (C 6 h 5 o 7 ) 2 2H 2 O, with a purity of 98.0-100.5% or more (medicine and food grade), is a white crystalline powder. It is a smart food additive for zinc supplementation and a medicine for treating loss of appetite and dysplasia. However, because it is insoluble in water, it is difficult for humans and animals to absorb. restrict its use. [0003] The main function of ascorbic acid (abbreviated as Vc, also known as vitamin C) is to improve immunity, prevent cancer, heart disease, stroke, protect teeth and gums, etc. The reductive properties of Vc can eliminate the nitroso and free radicals that cause canc...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C07D307/62C07C59/265C07C51/41A61K31/375A61K31/194A23L33/10A23L3/3562A61P35/00A61P1/14A61P1/00A61P11/00A61P11/06A61P1/16A61P29/00A61P9/12A23L33/00
CPCC07D307/62Y02A40/90
Inventor 李玉成
Owner 李玉成
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