The invention discloses a
thermal insulation multiphase
ceramic fiber aerogel used in an ultrahigh temperature environment of 1800 DEG C and a preparation method of the
thermal insulation multiphase
ceramic fiber aerogel. The preparation method comprises the following steps: mixing basic
zirconium carbonate, glacial
acetic acid and a
yttrium source according to a specific
molar ratio to prepare a
zirconium precursor solution; the preparation method comprises the following steps: adding an aluminum source and a
silicon source into a
solvent according to a specific
molar ratio, completely dissolving to obtain a
silicon-aluminum solution, condensing and refluxing until the solution is completely clarified to prepare a
silicon-aluminum precursor solution, mixing the silicon-aluminum precursor solution with the silicon-aluminum precursor solution according to a specific
molar ratio, solating to obtain a
zirconium-silicon-aluminum ternary
sol, adding a
spinning aid into the zirconium-silicon-aluminum ternary
sol to obtain a zirconium-aluminum-silicon ternary
spinning solution, and carrying out
spinning on the zirconium-silicon-aluminum ternary spinning solution to obtain the zirconium-silicon-aluminum ternary spinning solution. And carrying out electrostatic spinning or centrifugal spinning on the zirconium-aluminum-silicon ternary spinning solution to obtain a zirconium-aluminum-silicon
fiber aerogel precursor, collecting the zirconium-aluminum-silicon fiber aerogel precursor, heating to 1000-1300 DEG C, carrying out heat preservation, and cooling along with a furnace to obtain the aluminum
oxide-
zirconium oxide-
mullite fiber
ceramic aerogel with a three-dimensional structure. The aerogel prepared by the method is good in flexibility and has a good three-dimensional pore structure, and the fiber surface is smooth.