Adhesive for polarizing plate, polarizing plate including adhesive layer, and liquid crystal display
An adhesive layer, liquid crystal display panel technology, applied in the directions of non-polymer adhesive additives, adhesive types, adhesive additives, etc., can solve the problem of low water vapor transmission rate, micro-bubble and durability deterioration, etc. question
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Examples
Embodiment 1
[0100] 100 parts by weight of (A1) (meth)acrylic acid copolymer, 0.5 parts by weight of (B1) curing agent and 0.16 parts by weight of (B2) curing agent were introduced into 20 parts by weight of methyl ethyl ketone, followed by stirring at 25°C 5 minutes. 0.35 parts by weight of a silane coupling agent was added to the mixture, followed by stirring at 25° C. for 5 minutes, thereby preparing an adhesive for a polarizing plate.
Embodiment 2 to 4 and comparative example 1
[0102] An adhesive for a polarizing plate was prepared in the same manner as in Example 1, except that a curing agent was added in the amount listed in Table 1 (unit: parts by weight based on solid content). The minimum storage modulus of the adhesive layer was obtained by measuring each prepared adhesive by the method described below.
[0103] Table 1
[0104]
experiment example
[0105] Experimental Example: Property Evaluation of Adhesives for Polarizing Plates
[0106] The following properties of the adhesives for polarizing plates prepared in Examples and Comparative Examples were evaluated. The results are shown in Tables 2 and 3.
[0107] Methods of property evaluation
[0108] (1) Storage modulus (Pa): Each prepared adhesive for polarizing plates is coated on a polyethylene terephthalate release film, followed by drying at 90° C. for 4 minutes, thereby An adhesive sheet having a 20 μm thick adhesive layer was prepared. The adhesive layer was left at 35° C. and 45% RH for 3 days to cure the adhesive layer. Several cured adhesive layers were stacked on each other to form a 1 mm thick adhesive sheet, which was then cut into circular samples with a diameter of 8 mm. by at 85°C and about 10 -3 rad / s to about 10 2 The frequency sweep test was carried out at a frequency of rad / s, and the storage modulus of the sample was measured using a storage...
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