A kind of preparation method of anhydrous trehalose
An anhydrous trehalose, trehalose technology, applied in the directions of sugar derivative preparation, separation method, chemical instrument and method, can solve the problems of difficult popularization, high cost, difficult to completely remove crystal water, etc., and achieves steam saving and dehydration. The effect of thorough, omitting the crystallization step
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Embodiment 1
[0038] A preparation method of anhydrous trehalose, comprising the steps of:
[0039] (1) Using maltose syrup with a concentration of 90% as raw material, after 24 hours of conversion by immobilized trehalose synthase, a reaction solution containing 50wt% trehalose was obtained; the pH of the reaction solution was controlled at 4.2-4.7, 58°C, and 15U of glucoamylase was added / mL, keep warm for 10h, then raise the temperature to 80°C, keep warm for 10min, and filter to obtain trehalose crude solution;
[0040] Add 1wt% activated carbon to the prepared trehalose crude enzyme solution, keep the temperature at 65°C for 15 minutes, filter and desalt the ion exchange system, control the flow rate of ion exchange to 500kg / h, and the temperature at 30°C to make the feed liquid clear Transparent, no smell, light transmittance ≥ 95%;
[0041] (2) After concentrating the decolorized trehalose crude liquid obtained in step (1) to a total sugar content of 50 wt%, a trehalose purified liq...
Embodiment 2
[0045] A preparation method of anhydrous trehalose, comprising the steps of:
[0046] (1) Using maltose syrup with a concentration of 90% as raw material, after 48 hours of conversion by immobilized trehalose synthase, a reaction solution containing 65wt% trehalose was obtained; the pH of the reaction solution was controlled at 4.2-4.7 and 62°C, and 30 U of glucoamylase was added / mL, keep warm for 15h, then raise the temperature to 100°C, keep warm for 30min, and filter to obtain trehalose crude solution;
[0047] Add 3wt% activated carbon to the prepared trehalose crude enzyme solution, keep the temperature at 100°C for 30 minutes, filter and desalt the ion exchange system, control the flow rate of ion exchange at 1000kg / h, and the temperature at 55°C to make the feed liquid clear Transparent, no smell, light transmittance ≥ 95%;
[0048] (2) After concentrating the decolorized trehalose crude liquid obtained in step (1) to a total sugar content of 60 wt%, a trehalose purif...
Embodiment 3
[0052] A preparation method of anhydrous trehalose, comprising the steps of:
[0053] (1) Using maltose syrup with a concentration of 90% as raw material, after 36 hours of conversion by immobilized trehalose synthase, a reaction solution containing 60wt% trehalose was obtained; the pH of the reaction solution was controlled at 4.2-4.7 and 60°C, and 25 U of glucoamylase was added / mL, keep warm for 12h, then raise the temperature to 90°C, keep warm for 20min, and filter to obtain trehalose crude solution;
[0054] Add 2wt% activated carbon to the prepared trehalose crude enzyme solution, keep the temperature at 80°C for 20 minutes, filter and desalt the ion exchange system, control the flow rate of ion exchange at 800kg / h, and the temperature at 40°C to make the feed liquid clear Transparent, no smell, light transmittance ≥ 95%;
[0055] (2) After concentrating the decolorized trehalose crude liquid obtained in step (1) to a sugar content of 60 wt%, enter the simulated moving...
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