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Method for quickly preparing carbon quantum dots emitting blue light and carbon quantum dots emitting green light

A technology of green light carbon quantum and carbon quantum dots, which is applied in chemical instruments and methods, luminescent materials, nanotechnology for materials and surface science, etc., can solve the problems of complex preparation process, low product purity, long cycle, etc. Achieve the effects of good water solubility, good product purity and fast preparation speed

Active Publication Date: 2015-04-22
TAIYUAN UNIV OF TECH
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  • Abstract
  • Description
  • Claims
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Problems solved by technology

[0003] Ordinary quantum dot materials mostly contain heavy metal elements, which are highly toxic; carbon quantum dots, as a fluorescent nanomaterial, mainly contain carbon, which is one of the most abundant elements in nature, so the cost of carbon quantum dots is relatively low ; Carbon quantum dots have down-conversion and up-conversion fluorescence properties, good chemical stability, good biocompatibility and low toxicity, and have broad application prospects in biological imaging, medical diagnosis, catalysis and photovoltaic devices; currently synthetic carbon There are many methods for quantum dots, but most of them have complex preparation process, long cycle, low product purity, and many disadvantages

Method used

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  • Method for quickly preparing carbon quantum dots emitting blue light and carbon quantum dots emitting green light
  • Method for quickly preparing carbon quantum dots emitting blue light and carbon quantum dots emitting green light
  • Method for quickly preparing carbon quantum dots emitting blue light and carbon quantum dots emitting green light

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Embodiment Construction

[0055] The present invention will be further described below in conjunction with accompanying drawing:

[0056] figure 1 As shown, the state diagram of the carbon quantum dot solution is prepared for hydrothermal synthesis. The position and connection relationship of each part must be correct, and the ratio should be adjusted according to the amount and operation in order.

[0057] Quantities of the chemical substances used in the preparation are determined according to a preset range, with grams and milliliters as measurement units.

[0058] The hydrothermal synthesis of carbon quantum dot solution is carried out in a heating furnace and a reaction kettle, and is completed under heating; the heating furnace is a vertical type, and the upper part of the heating furnace 1 is the furnace cover 2, and the lower part is the first electric control box 3. In the heating furnace 1 is a furnace cavity 13, and at the bottom of the furnace cavity 13 is a first workbench 4. A reaction k...

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Abstract

The invention relates to a method for quickly preparing carbon quantum dots emitting blue light and carbon quantum dots emitting green light. According to the method, an environmentally-friendly hydrothermal synthesis method is adopted, L-ascorbic acid and ethidene diamine serve as raw materials, deionized water serves as solvent, the carbon quantum dots emitting the blue light and the carbon quantum dots emitting the green light are formed by quick synthesis of the L-ascorbic acid at different temperatures, the purity of products reaches 99%, the water solubility reaches 99.5%, the particle diameter of the carbon quantum dots emitting the blue light is smaller than or equal to 6 nm, the particle diameter of the carbon quantum dots emitting the green light is smaller than or equal to 6.2 nm, and the carbon quantum dots are good in dispersity, good in water solubility, good in fluorescence, capable of being applied to fluorescence probes, biomedical imaging, printing inks and photovoltaic devices; the preparation method is advanced in process, precise and detailed in data, high in preparation speed, good in product purity and stable in light-emitting performance and is a very ideal method for quickly preparing the carbon quantum dots emitting the blue light and the carbon quantum dots emitting the green light.

Description

technical field [0001] The invention relates to a rapid preparation method of carbon quantum dots emitting blue light and green light, and belongs to the technical field of rapid preparation and application of blue light and green light carbon quantum dots. Background technique [0002] Fluorescent carbon nanomaterials have good application prospects due to their unique optical properties, low toxicity and good biocompatibility. Carbon quantum dots are the most important fluorescent carbon materials in fluorescent carbon nanomaterials, and their morphology is zero. Dimensional nanoparticles, similar in size to quantum dots, smaller than 10nm. [0003] Ordinary quantum dot materials mostly contain heavy metal elements, which are highly toxic; carbon quantum dots, as a fluorescent nanomaterial, mainly contain carbon, which is one of the most abundant elements in nature, so the cost of carbon quantum dots is relatively low ; Carbon quantum dots have down-conversion and up-conv...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C09K11/65B82Y30/00B82Y40/00B82Y20/00
Inventor 刘旭光冯晓婷杨永珍张漪何玉珩
Owner TAIYUAN UNIV OF TECH
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