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Cellulose fiber in-situ mineralization deep water-saving emission reduction dyeing post-treatment method and auxiliaries

A cellulose fiber, in-situ mineralization technology, applied in the direction of dyeing, textile and papermaking, etc., can solve the problems of high water consumption, high pollution, and no new dyeing technology found in cellulose fiber dyeing and processing.

Active Publication Date: 2017-01-04
XI'AN POLYTECHNIC UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

However, after dyeing, there is still a certain amount of residual dye in the dyeing residual bath and on the dyed fiber, and the discharge of pollutants and a large number of soaping and washing steps are indispensable.
Therefore, the above studies still cannot fundamentally solve the problems of high water consumption and high pollution in cellulose fiber dyeing and processing.
[0006] To sum up, for the dyeing process of cellulose fiber, a feasible new dyeing technology for deep water saving and emission reduction has not been found at home and abroad.

Method used

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  • Cellulose fiber in-situ mineralization deep water-saving emission reduction dyeing post-treatment method and auxiliaries
  • Cellulose fiber in-situ mineralization deep water-saving emission reduction dyeing post-treatment method and auxiliaries

Examples

Experimental program
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Effect test

preparation example Construction

[0071] The preparation method of cellulose fiber post-dyeing treatment auxiliary agent XAC specifically implements according to the following steps:

[0072] Step 1, take the following raw materials respectively according to the mass percentage:

[0073] Polyacrylamide 0.001% to 5%, polyaluminum sulfate or polyaluminum chloride 0.001% to 2.5%, dodecyl dimethyl benzyl ammonium chloride 5.0% to 40%, dioctadecyl-methyl benzyl Ammonium chloride 0.1%~5.0%, Dioctadecyldimethylammonium chloride 0.05%~2.0%, Fatty alcohol polyoxyethylene ether 10%~30%, Purified water 15.5%~84.848%, the above components The sum of the contents is 100%;

[0074] Step 2, heating the purified water weighed in step 1 to 40°C to 50°C;

[0075] Step 3, polyacrylamide, polyaluminum sulfate or polyaluminum chloride, dodecyl dimethyl benzyl ammonium chloride, dioctadecyl-methyl benzyl ammonium chloride, Dioctadecyldimethylammonium chloride and fatty alcohol polyoxyethylene ether are added together to the puri...

Embodiment 1

[0108] Cellulose fiber post-dyeing treatment aid XAC, composed of the following raw materials by mass percentage: polyacrylamide 1%, polyaluminum sulfate 1.5%, dodecyl dimethyl benzyl ammonium chloride 6.0%, dioctadecyl - 0.5% of methyl benzyl ammonium chloride, 1.0% of dioctadecyl dimethyl ammonium chloride, 15% of flat plus O, 75% of purified water, the total content of the above components is 100%;

[0109] The preparation method of XAC, the post-processing auxiliary agent for cellulose fiber dyeing: Weigh the following raw materials according to the mass percentage: polyacrylamide 1%, polyaluminum sulfate 1.5%, dodecyl dimethyl benzyl ammonium chloride 6.0%, bis 0.5% octadecyl-methylbenzyl ammonium chloride, 1.0% dioctadecyl dimethyl ammonium chloride, 15% Ping Pinga O, 75% pure water, the total content of the above components is 100%; Heat the weighed pure water to 40°C; weigh the weighed polyacrylamide, polyaluminum sulfate, dodecyldimethylbenzylammonium chloride, diocta...

Embodiment 2

[0116] The post-treatment auxiliary XAC for cellulose fiber dyeing is composed of the following raw materials by mass percentage: polyacrylamide 1.5%, polyaluminum sulfate 2.0%, dodecyl dimethyl benzyl ammonium chloride 5.0%, dioctadecyl - 0.8% of methyl benzyl ammonium chloride, 1.5% of dioctadecyl dimethyl ammonium chloride, 12% of flat plus O, 77.2% of purified water, the total content of the above components is 100%;

[0117] The preparation method of XAC, the post-treatment auxiliary agent for cellulose fiber dyeing: Weigh the following raw materials according to the mass percentage: polyacrylamide 1.5%, polyaluminum sulfate 2.0%, dodecyl dimethyl benzyl ammonium chloride 5.0%, bis 0.8% of octadecyl-methylbenzyl ammonium chloride, 1.5% of dioctadecyl dimethyl ammonium chloride, 12% of Ping Pinga O, 77.2% of pure water, the total content of the above components is 100%; Heat the weighed pure water to 40°C; weigh the weighed polyacrylamide, polyaluminum sulfate, dodecyldime...

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Abstract

The invention discloses a cellulosic fiber in-situ mineralization deep water-saving and emission reduction dyeing aftertreatment method which comprises the following steps: firstly, putting a fabric to be dyed into dyeing equipment, adding dyeing water into the dyeing equipment, and keeping circulation of a dye bath; performing dyeing processing on the fabric to be dyed by using a common deying method for the cellulosic fiber, and after dyeing is completed, retaining the residual dyeing liquid; further simultaneously performing in-situ mineralization treatment on the residual dyeing liquid obtained after cellulosic fiber dyeing processing and the dyed fabric by using cellulosic fiber aftertreatment additives XAC, XBC and XYC; storing the residual dyeing liquid obtained after the mineralization treatment as later dyeing water; dehydrating and drying the dyed fabric, thereby completing dyeing and aftertreatment on the fabric. The invention further discloses the cellulosic fiber dyeing aftertreatment additives XAC, XBC and XYC. By adopting the dyeing aftertreatment method disclosed by the invention, the water consumption problem and the wastewater discharge problem in the cellulosic fiber dyeing processing can be fundamentally solved.

Description

technical field [0001] The invention belongs to the technical field of textile dyeing and finishing, and specifically relates to the in-situ mineralization and deep water-saving and emission-reducing post-dyeing treatment method for the dyeing residual bath and dyed fibers after dyeing of cellulose fibers. The invention also relates to the above-mentioned in-situ The cellulose fiber dyeing post-treatment auxiliary agent XAC, the cellulose fiber dyeing post-treatment auxiliary agent XBC, and the cellulose fiber dyeing post-treatment auxiliary agent XYC involved in the mineralization and deep water-saving and emission-reducing dyeing post-treatment method. Background technique [0002] A certain amount of residual dyes and residual dyeing auxiliaries often exist in the dyeing residual bath of cellulose fibers after dyeing, and a certain amount of residual dyes also exist on the dyed fibers. In the traditional dyeing process of cellulose fiber, the above-mentioned dyeing residu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): D06P3/60D06P5/08D06P5/10D06P5/06
Inventor 邢建伟沈兰萍徐成书赵航欧阳磊袁利王卓睿苏广召周梦宇吴钦任燕王志刚
Owner XI'AN POLYTECHNIC UNIVERSITY
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