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31results about How to "Save water for dyeing" patented technology

Reactive dye ecological dyeing method of silk fabrics

The invention provides a reactive dye ecological dyeing method of silk fabrics, which comprises the following steps of: (1) even dyeing: using reactive dye and decamethyl cyclopenta siloxane (D5) according to the mass ratio of 1:10 to 50 to prepare a reactive dye/D5 suspending dispersed liquid; padding the silk fabrics in 30 to 90 g/l of sodium bicarbonate solution; and dyeing the silk fabrics in the reactive dye/D5 suspending dispersed liquid with the rolling liquid rate of 160 to 200% at room temperature for 25 to 35 minutes, wherein the rolling liquid rate is used for ensuring even dyeing of the silk fabrics; and (2) color fixing: heating a mixture system obtained from the step (1) to 40 to 50 DEG C, and keeping the temperature for 20 to 30 minutes; then heating to 70 to 90 DEG C, and keeping the temperature for 20 to 30 minutes; and taking the silk fabrics out, and performing soap boiling. In the process of dyeing provided by the invention, an electrolyte is not added for dyeing acceleration, the dyeing rate of the dye is close to 100%, the fixing rate is higher than that of traditional bath dyeing, and the fastness of the fabrics is good after dyeing. Because the electrolyte is not needed for dyeing acceleration, the burden of treating dyeing waste water is effectively reduced, and the ecological environment is protected.
Owner:ZHEJIANG SCI-TECH UNIV

Cellulosic fiber in-situ mineralization deep water-saving and emission reduction dyeing aftertreatment method and additive

ActiveCN104695253AReduced dichromate indexFully eliminateDyeing processWastewaterCellulose fiber
The invention discloses a cellulosic fiber in-situ mineralization deep water-saving and emission reduction dyeing aftertreatment method which comprises the following steps: firstly, putting a fabric to be dyed into dyeing equipment, adding dyeing water into the dyeing equipment, and keeping circulation of a dye bath; performing dyeing processing on the fabric to be dyed by using a common deying method for the cellulosic fiber, and after dyeing is completed, retaining the residual dyeing liquid; further simultaneously performing in-situ mineralization treatment on the residual dyeing liquid obtained after cellulosic fiber dyeing processing and the dyed fabric by using cellulosic fiber aftertreatment additives XAC, XBC and XYC; storing the residual dyeing liquid obtained after the mineralization treatment as later dyeing water; dehydrating and drying the dyed fabric, thereby completing dyeing and aftertreatment on the fabric. The invention further discloses the cellulosic fiber dyeing aftertreatment additives XAC, XBC and XYC. By adopting the dyeing aftertreatment method disclosed by the invention, the water consumption problem and the wastewater discharge problem in the cellulosic fiber dyeing processing can be fundamentally solved.
Owner:XI'AN POLYTECHNIC UNIVERSITY

Dyeing process of fire retardant fibers

The invention aims at providing a dyeing process of fire retardant fibers. The dyeing process comprises the following steps: step 1, desizing: adding the fire retardant fibers into a desizing eater solution at 50-60 DEG C, keeping the heat and washing with water; step 2, rinsing: adding the fire retardant fibers subjected to the desizing into a rising water solution at 95-100 DEG C, keeping the heat and washing with the water; step 3, dehairing: taking the rinsed fire retardant fibers and removing hairs on the surfaces of the fire retardant fibers; step 4, dyeing: taking the unhaired fire retardant fibers and adding the unhaired fire retardant fibers into water at 15-35 DEG C; gradually heating a water bath to 100-102 DEG C; adding dyestuff when the water bath is 68-71 DEG C and adding a dyestuff auxiliary agent when the water bath is 95-100 DEG C; keeping the heat at 100-102 DEG C for 0.5-1 hour; gradually heating the water bath to 130-135 DEG C and keeping the heat at 130-135 DEG C for 0.5-1 hour; gradually cooling the water bath to 75-80 DEG C; taking out the fire retardant fibers and soaping at 75-80 DEG C for 0.1-0.5 hour; and step 5, finishing: taking the dyed fire retardant fibers and sequentially carrying out air finishing and full decatizing finishing on the dyed fire retardant fibers. The dyeing process has the advantage that the dyeing effect is improved.
Owner:HANGZHOU ZHUODA PRINTING & DYEING CO LTD

Microcapsule dyeing method of poly lactic acid fibers and/or poly lactic acid fiber product

The present invention relates to a microcapsule dyeing method of poly lactic acid fibers and / or a poly lactic acid fiber product. The method comprises: (1) weighing disperse dye microcapsules according to 0.1-10% (o.w.f.), adopting a HAc aqueous solution as a dyeing solution, weighing and taking the dyeing solution according to a bath ratio of 15-60:1, and carrying out dyeing for the poly lactic acid fibers and / or the poly lactic acid fiber product; (2) carrying out acid washing for the dyed poly lactic acid fibers and / or the poly lactic acid fiber product, then washing by clear water, and drying to obtain the product; or filtering the resulting waste water from the step (1) to obtain the microcapsule-free dyeing bath, soaking the dyed poly lactic acid fibers and / or the poly lactic acid fiber product into the resulting microcapsule-free dyeing bath, carrying out a thermal insulation treatment for 10-20 minutes at a temperature of 70-110 DEG C, then washing by clear water, and drying to obtain the product. The method of the present invention has the following advantages that: the dyeing process is simple; the dyeing time is short; the reductive cleaning treatment is saved; the dyeing solution cleaning is easy to treat; the purposes of environmental protection and cost saving are achieved; the damage on the PLA fibers is low, the tint is dark after dyeing, and the color fastnessis high.
Owner:DONGHUA UNIV

In-situ mineralization and water-saving emission-reduction dyeing post-treatment method for polyacrylonitrile fibers and auxiliary agents

ActiveCN104711877AReduced dichromate indexFully eliminateDyeing processWater savingWastewater
The invention discloses an in-situ mineralization and water-saving emission-reduction dyeing post-treatment method for polyacrylonitrile fibers. The method comprises the following steps: putting a to-be-dyed textile into dyeing equipment, adding dyeing water, keeping dye bath recycling, and making preparations before dyeing; performing dyeing processing on the to-be-dyed textile with a general polyacrylonitrile fiber dyeing method, and not discharging dyeing residual liquid after finishing dyeing; performing mineralization treatment on the dyed textile by utilizing polyacrylonitrile fiber dyeing post-treatment auxiliary agents XAQ, XBQ and XYQ; performing treatment on the obtained residual dyeing bath and the dyed textile, and finishing the whole dyeing post-treatment process. The invention further relates to respective formulae and preparation methods of the polyacrylonitrile fiber dyeing post-treatment auxiliary agents XAQ, XBQ and XYQ. The in-situ mineralization and deep water-saving emission-reduction dyeing post-treatment method for the polyacrylonitrile fibers and the auxiliary agents solve problems of high water consumption and high wastewater discharge amount in a polyacrylonitrile fiber dyeing processing process.
Owner:XI'AN POLYTECHNIC UNIVERSITY

In-situ mineralization of polyacrylonitrile fiber, water-saving and emission-reduction dyeing post-treatment method and auxiliaries

The invention discloses an in-situ mineralization and water-saving emission-reduction dyeing post-treatment method for polyacrylonitrile fibers. The method comprises the following steps: putting a to-be-dyed textile into dyeing equipment, adding dyeing water, keeping dye bath recycling, and making preparations before dyeing; performing dyeing processing on the to-be-dyed textile with a general polyacrylonitrile fiber dyeing method, and not discharging dyeing residual liquid after finishing dyeing; performing mineralization treatment on the dyed textile by utilizing polyacrylonitrile fiber dyeing post-treatment auxiliary agents XAQ, XBQ and XYQ; performing treatment on the obtained residual dyeing bath and the dyed textile, and finishing the whole dyeing post-treatment process. The invention further relates to respective formulae and preparation methods of the polyacrylonitrile fiber dyeing post-treatment auxiliary agents XAQ, XBQ and XYQ. The in-situ mineralization and deep water-saving emission-reduction dyeing post-treatment method for the polyacrylonitrile fibers and the auxiliary agents solve problems of high water consumption and high wastewater discharge amount in a polyacrylonitrile fiber dyeing processing process.
Owner:XI'AN POLYTECHNIC UNIVERSITY

Device and method for recovering acid dye residue and heat energy

The invention discloses an acid dye dyeing residue and heat energy recycling device and method. The acid dye dyeing residue and heat energy recycling device and method comprises a dye vat. The dye vat is connected with a vessel, wherein the volume of the vessel is greater than or equal to the dye vat. A heat exchanging coil pipe is arranged in the vessel, one end of the heat exchanging coil pipe is connected with a water inlet port, and the other end of the heat exchanging coil pipe is connected with the dye vat. Longitudinal sliding rails are arranged in the vessel, and sliding blocks are arranged on the sliding rails. A linear motor is arranged in the vessel, an output shaft of the linear motor is fixedly connected with the heat exchanging coil pipe. According to the acid dye dyeing residue and heat energy recycling device and method, by collecting the dyeing residue, the heat energy of the dyeing residue can be utilized for hot water washing, soaping and fixation process after dyeing, and moreover, by adding water, leveling agent, acid and dye into the dyeing residue until the dyeing residue returns back to the pre-dyeing status, so that recycling using of the dyeing residue is realized. According to the acid dye dyeing residue and heat energy recycling device and method, dosage of the leveling agent, the acid and the dye are decreased, dyeing cost is reduced, and dyeing processing efficiency are is improved.
Owner:贵州鼎盛服饰有限公司

A dyeing process of flame-retardant blended fiber

The invention aims to provide a dyeing process of flame-retardant mixed fiber. The dyeing process includes following steps: adding the flame-retardant mixed fiber into a desizing water solution of 50-60 DEG C, holding the temperature, and washing with water at 50-70 DEG C; adding the flame-retardant mixed fiber that is desized into a rinsing water solution of 95-100 DEG C, holding the temperature, and washing with water at 50-70 DEG C; unhairing; adding the flame-retardant mixed fiber that is unhaired into water of 15-35 DEG C, rising the temperature to 100-102 DEG C, adding dye at 68-71 DEG C, adding a dye auxiliary at 95-100 DEG C, and holding the temperature at 100-102 DEG C; rising the temperature to 130-135 DEG C, and holding the temperature at 130-135 DEG C; lowering the temperature to 75-80 DEG C; taking out the flame-retardant mixed fiber, and soaping the flame-retardant mixed fiber at 75-80 DEG C; taking the flame-retardant mixed fiber dyed for the first time, padding the flame-retardant mixed fiber in dye liquid, and air-drying at high temperature; padding the flame-retardant mixed fiber in color fixing liquid, and performing saturated steaming at high temperature; subjecting the flame-retardant mixed fiber after saturated steaming to water washing at 10-15 DEG C, acetic acid neutralizing, soaping at 85-90 DEG C and water washing at 15-35 DEG C sequentially; taking the flame-retardant mixed fiber after being dyed, and subjecting the flame-retardant mixed fiber to air finishing and full decatizing sequentially. The dyeing process has the advantage that dyeing effect is improved.
Owner:HANGZHOU ZHUODA PRINTING & DYEING CO LTD

Cellulose fiber in-situ mineralization deep water-saving emission reduction dyeing post-treatment method and auxiliaries

ActiveCN104695253BReduced dichromate indexFully eliminateDyeing processWastewaterCellulose fiber
The invention discloses a cellulosic fiber in-situ mineralization deep water-saving and emission reduction dyeing aftertreatment method which comprises the following steps: firstly, putting a fabric to be dyed into dyeing equipment, adding dyeing water into the dyeing equipment, and keeping circulation of a dye bath; performing dyeing processing on the fabric to be dyed by using a common deying method for the cellulosic fiber, and after dyeing is completed, retaining the residual dyeing liquid; further simultaneously performing in-situ mineralization treatment on the residual dyeing liquid obtained after cellulosic fiber dyeing processing and the dyed fabric by using cellulosic fiber aftertreatment additives XAC, XBC and XYC; storing the residual dyeing liquid obtained after the mineralization treatment as later dyeing water; dehydrating and drying the dyed fabric, thereby completing dyeing and aftertreatment on the fabric. The invention further discloses the cellulosic fiber dyeing aftertreatment additives XAC, XBC and XYC. By adopting the dyeing aftertreatment method disclosed by the invention, the water consumption problem and the wastewater discharge problem in the cellulosic fiber dyeing processing can be fundamentally solved.
Owner:XI'AN POLYTECHNIC UNIVERSITY

Microcapsule dyeing method of poly lactic acid fibers and/or poly lactic acid fiber product

The present invention relates to a microcapsule dyeing method of poly lactic acid fibers and / or a poly lactic acid fiber product. The method comprises: (1) weighing disperse dye microcapsules according to 0.1-10% (o.w.f.), adopting a HAc aqueous solution as a dyeing solution, weighing and taking the dyeing solution according to a bath ratio of 15-60:1, and carrying out dyeing for the poly lactic acid fibers and / or the poly lactic acid fiber product; (2) carrying out acid washing for the dyed poly lactic acid fibers and / or the poly lactic acid fiber product, then washing by clear water, and drying to obtain the product; or filtering the resulting waste water from the step (1) to obtain the microcapsule-free dyeing bath, soaking the dyed poly lactic acid fibers and / or the poly lactic acid fiber product into the resulting microcapsule-free dyeing bath, carrying out a thermal insulation treatment for 10-20 minutes at a temperature of 70-110 DEG C, then washing by clear water, and drying to obtain the product. The method of the present invention has the following advantages that: the dyeing process is simple; the dyeing time is short; the reductive cleaning treatment is saved; the dyeing solution cleaning is easy to treat; the purposes of environmental protection and cost saving are achieved; the damage on the PLA fibers is low, the tint is dark after dyeing, and the color fastness is high.
Owner:DONGHUA UNIV

In-situ mineralization of disperse dyes, deep water saving and emission reduction dyeing post-treatment method and auxiliaries

The invention discloses a dispersed dye in-situ mineralization and deep water conservation emission reduction dyeing aftertreatment method which comprises the following steps: firstly, putting a fabric to be dyed into dyeing equipment, adding dyeing water into the dyeing equipment, and keeping circulation of a dye bath; performing conventional dyeing processing on the fabric to be dyed in the dyeing equipment by using dispersed dye and using a high-temperature high-pressure dyeing method, and after dyeing is completed, retaining the residual dyeing bath; further simultaneously performing in-situ mineralization treatment on the residual dyeing bath and the dyed fabric; finally storing the residual dyeing bath obtained after the treatment as later dyeing water, and dehydrating and drying the dyed fabric, thereby completing the whole aftertreatment process. The invention further discloses three additives used in the dyeing aftertreatment method. By adopting the aftertreatment method disclosed by the invention, later reduction washing and water washing after dyeing can be avoided, the residual dyeing liquid after the in-situ mineralization treatment can be further reused in later dyeing treatment, and thus the water consumption and the pollutant discharge amount of the whole dyeing treatment can be greatly reduced.
Owner:XI'AN POLYTECHNIC UNIVERSITY
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