In-situ mineralization and water-saving emission-reduction dyeing post-treatment method for polyacrylonitrile fibers and auxiliary agents

A technology of polyacrylonitrile fiber and in-situ mineralization is applied in the field of textile dyeing and finishing, which can solve the problems of large water consumption and large waste water discharge.

Active Publication Date: 2015-06-17
XI'AN POLYTECHNIC UNIVERSITY
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0007] The first purpose of the present invention is to provide in-situ mineralization of polyacrylonitrile fibers, deep water saving and emission reduction post-dyein

Method used

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  • In-situ mineralization and water-saving emission-reduction dyeing post-treatment method for polyacrylonitrile fibers and auxiliary agents
  • In-situ mineralization and water-saving emission-reduction dyeing post-treatment method for polyacrylonitrile fibers and auxiliary agents
  • In-situ mineralization and water-saving emission-reduction dyeing post-treatment method for polyacrylonitrile fibers and auxiliary agents

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Experimental program
Comparison scheme
Effect test

Embodiment 1

[0118] Polyacrylonitrile fiber dyeing post-treatment auxiliary XAQ, composed of the following raw materials by mass percentage: polyacrylamide 1%, polyaluminum sulfate 1.5%, dodecyl dimethyl benzyl ammonium chloride 6.0%, dioctadecane Base-methyl benzyl ammonium chloride 0.5%, dioctadecyl dimethyl ammonium chloride 1.0%, Pingpingjiao 15%, purified water 75%, the total content of the above components is 100%;

[0119] The preparation method of XAQ, the post-processing auxiliary agent for polyacrylonitrile fiber dyeing: Weigh the following raw materials according to mass percentage: polyacrylamide 1%, polyaluminum sulfate 1.5%, dodecyl dimethyl benzyl ammonium chloride 6.0%, 0.5% dioctadecyl-methyl benzyl ammonium chloride, 1.0% dioctadecyl dimethyl ammonium chloride, 15% Ping Pinga O, 75% pure water, the total content of the above components is 100%; The weighed polyacrylamide, polyaluminum sulfate, dodecyl dimethyl benzyl ammonium chloride, dioctadecyl-methyl benzyl ammonium c...

Embodiment 2

[0126] Polyacrylonitrile fiber dyeing post-treatment auxiliary XAQ, composed of the following raw materials by mass percentage: polyacrylamide 1.5%, polyaluminum sulfate 2.0%, dodecyl dimethyl benzyl ammonium chloride 5.0%, dioctadecane Base-methyl benzyl ammonium chloride 0.8%, dioctadecyl dimethyl ammonium chloride 1.5%, Pingpingjiao 12%, purified water 77.2%, the total content of the above components is 100%;

[0127] The preparation method of XAQ, the post-processing auxiliary agent for polyacrylonitrile fiber dyeing: Weigh the following raw materials according to mass percentage: polyacrylamide 1.5%, polyaluminum sulfate 2.0%, dodecyl dimethyl benzyl ammonium chloride 5.0%, 0.8% dioctadecyl-methylbenzyl ammonium chloride, 1.5% dioctadecyldimethyl ammonium chloride, 12% Ping Pinga O, 77.2% pure water, the total content of the above components is 100%; The weighed polyacrylamide, polyaluminum sulfate, dodecyl dimethyl benzyl ammonium chloride, dioctadecyl-methyl benzyl ammo...

Embodiment 3

[0134] Polyacrylonitrile fiber dyeing post-treatment auxiliary XAQ, composed of the following raw materials by mass percentage: polyacrylamide 1.0%, polyaluminum sulfate 1.3%, dodecyl dimethyl benzyl ammonium chloride 3.0%, dioctadecane Base-methyl benzyl ammonium chloride 1.0%, dioctadecyl dimethyl ammonium chloride 1.2%, Pingpingjiao 10%, purified water 82.5%, the total content of the above components is 100%;

[0135] The preparation method of polyacrylonitrile fiber dyeing post-treatment auxiliary agent XAQ: Weigh the following raw materials according to mass percentage: polyacrylamide 1.0%, polyaluminum sulfate 1.3%, dodecyl dimethyl benzyl ammonium chloride 3.0%, 1.0% dioctadecyl-methylbenzyl ammonium chloride, 1.2% dioctadecyldimethyl ammonium chloride, 10% Ping Pinga O, 82.5% purified water, the total content of the above components is 100%; The weighed polyacrylamide, polyaluminum sulfate, dodecyl dimethyl benzyl ammonium chloride, dioctadecyl-methyl benzyl ammonium c...

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Abstract

The invention discloses an in-situ mineralization and water-saving emission-reduction dyeing post-treatment method for polyacrylonitrile fibers. The method comprises the following steps: putting a to-be-dyed textile into dyeing equipment, adding dyeing water, keeping dye bath recycling, and making preparations before dyeing; performing dyeing processing on the to-be-dyed textile with a general polyacrylonitrile fiber dyeing method, and not discharging dyeing residual liquid after finishing dyeing; performing mineralization treatment on the dyed textile by utilizing polyacrylonitrile fiber dyeing post-treatment auxiliary agents XAQ, XBQ and XYQ; performing treatment on the obtained residual dyeing bath and the dyed textile, and finishing the whole dyeing post-treatment process. The invention further relates to respective formulae and preparation methods of the polyacrylonitrile fiber dyeing post-treatment auxiliary agents XAQ, XBQ and XYQ. The in-situ mineralization and deep water-saving emission-reduction dyeing post-treatment method for the polyacrylonitrile fibers and the auxiliary agents solve problems of high water consumption and high wastewater discharge amount in a polyacrylonitrile fiber dyeing processing process.

Description

technical field [0001] The invention belongs to the technical field of textile dyeing and finishing, and specifically relates to a method for in-situ mineralization and deep water-saving and emission-reducing post-dyeing treatment of the dyed residual bath and dyed fibers after dyeing of polyacrylonitrile fibers. The invention also relates to the above-mentioned dyeing method Three kinds of post-treatment auxiliaries XAQ, XBQ and XYQ used in the post-treatment method for polyacrylonitrile fiber dyeing. Background technique [0002] There is often a certain amount of residual dye and residual dyeing auxiliaries in the dyeing residual bath of polyacrylonitrile fiber after dyeing, and there is also a certain amount of residual dye on the dyed fiber. In the traditional dyeing process of polyacrylonitrile fibers, the above-mentioned residual dyeing bath must be discharged, resulting in high dyeing wastewater treatment costs, and there are hidden dangers of environmental pollution...

Claims

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Application Information

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IPC IPC(8): D06P5/02D06P5/10D06P5/08D06P5/06D06P5/04D06P3/70D06P1/00
Inventor 邢建伟沈兰萍徐成书袁利赵航苏广召欧阳磊王卓睿周梦宇吴钦任燕王志刚
Owner XI'AN POLYTECHNIC UNIVERSITY
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