Bioflavonoid Coating Materials
A technology of bioflavonoids and polymer materials, applied in the field of polymer materials, can solve the problems such as the application of bioflavonoid compositions that are not disclosed
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Embodiment 1
[0106] experimental method
[0107] Preparation of Citrox Precursor: Citrox HXT powder was dissolved in methanol. The precursors were formulated using either 10 wt% or 15 wt% Citrox in methanol.
[0108] Pretreatment of samples: Preliminary He / O with or without polyethylene terephthalate (PET) films and silicon wafers 2 Plasma pretreatment.
[0109] In atmospheric plasma jet processing systems (e.g. PlasmaStream TM ), 5% O in He was used through two rounds 2 The resulting plasma activated substrate. The applied plasma powder was 80%, the CNC speed was 7 mm / sec, and the distance from the substrate to the plasma jet orifice was 10 mm.
[0110] In reel-to-reel atmospheric plasmas (e.g. Labline TM In the case of system), an O2 containing 5% of He in 2 The processing chamber is passed three times to activate the substrate. The applied plasma powder was 1000 W and the sample was passed through the chamber at a speed of 1.5 m / sec.
[0111] Import into PlasmaStream using TM ...
Embodiment 2
[0155] Impregnation of polystyrene sheets with Citrox
[0156] Polystyrene sheets were treated using plasma immersion ion implantation (PIII) with nitrogen ions at an energy of 20 keV for 800 seconds to form a surface embedded with groups capable of covalently binding bioactive molecules (as in Bilek et al., PNAS, 08( 35):14405-14410, 2011, which is hereby incorporated by reference). PIII-treated and untreated sheets were incubated for 3 hours in tubes filled with Citrox concentrate (PHLC 45) or deionized water (for controls). Contains bioflavonoids in HPLC 45 or "Citrox BC" 45% (total composition of HPLC 45 / Citrox BC). The bioflavonoids were in admixture with biomass residues extracted from bitter oranges such as pectin, sugars and small amounts of organic acids (which constituted the remaining 55%). HPLC 45 is available from Exquim (a company of Grupo Ferrer) as Citrus BioflavonoidComplex 45% HPLC. After incubation, the sheets were washed thoroughly in the tubes with deio...
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