An electrochemical method for removing heavy metal cadmium in silkworm excrement
An electrochemical and heavy metal technology, applied to the removal of solid waste, can solve the problems of different migration speeds of heavy metal cations, heavy metals that cannot achieve the treatment effect, and different removal rates of heavy metals, so as to save electrolysis time, improve electrolysis efficiency, and treat fast effect
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Embodiment 1
[0028] The concentration of Cd contained in silkworm excrement in a certain place is 0.67mg / kg, respectively use 0.1mol / LEDTA, citric acid or acetic acid as the extractant, adjust the pH value to 2 with hydrochloric acid, and then enter the electrochemical treatment device with graphite as the electrode. After 10h electrochemical treatment, when the voltage gradient is 0.5V / cm, the removal rates of Cd in silkworm excrement are 82.0, 77.2 and 72.6% respectively; when the voltage gradient is 1.0V / cm, the removal rate of Cd in silkworm excrement The removal rates of Cd in silkworm excrement were 81.1, 75.3 and 77.2% respectively at a voltage gradient of 1.5V / cm. The concentration of remaining Cd in silkworm excrement is all lower than the limit value of 0.3mg / kg, which meets the green industry standard of foreign trade and economic cooperation of medicinal plants and preparations (green Chinese medicine standard WM / T2-2004).
Embodiment 2
[0030] The concentration of Cd contained in silkworm excrement in a certain place is 1.67mg / kg, respectively use 0.1mol / LEDTA, citric acid or acetic acid as the extractant, adjust the pH value to 4 with hydrochloric acid, enter the electrochemical treatment device with graphite as the electrode, and the voltage gradient is 0.5~1.5V / cm, the electrode plate spacing is 14cm, after 10h electrochemical treatment, when the voltage gradient is 0.5V / cm, the removal rates of Cd in silkworm excrement are 88.1, 86.7 and 81.1%; the voltage gradient is 1.0V / cm, the removal rates of Cd in silkworm excrement were 88.8, 81.0 and 81.1%; the voltage gradient was 1.5V / cm, and the removal rates of Cd in silkworm excrement were 89.3, 81.5 and 80.4%. The concentration of remaining Cd in silkworm excrement is all lower than the limit value of 0.3mg / kg, which meets the green industry standard of foreign trade and economic cooperation of medicinal plants and preparations (green Chinese medicine standa...
Embodiment 3
[0032] The concentration of Cd contained in silkworm excrement in a certain place is 0.67mg / kg, and 0.1mol / LEDTA, citric acid or acetic acid are used as the extractant respectively, and after the pH value is adjusted to 6 with hydrochloric acid, it enters the electrochemical treatment device with graphite as the electrode. The spacing is 14cm, after 10h electrochemical treatment, when the voltage gradient is 0.5V / cm, the removal rates of Cd in silkworm excrement are 79.6, 73.2 and 71.9% respectively; The removal rates were 79.6, 76.6 and 70.7%; the voltage gradient was 1.5V / cm, and the removal rates of Cd in silkworm excrement were 74.5, 69.0 and 63.4%. The concentration of remaining Cd in silkworm excrement is all lower than the limit value of 0.3mg / kg, which meets the green industry standard of foreign economic and trade of medicinal plants and preparations (green Chinese medicine standard WM / T2-2004).
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