A kind of inorganic flame-resistant paper and its preparation method and application
A technology of inorganic flame-resistant paper and inorganic filler, which is used in spinning solution preparation, textile and papermaking, fiber processing, etc., can solve problems such as low technical preparation efficiency, and achieve environmental pressure relief, good mechanical properties, and good chemical stability. Effect
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Embodiment 1
[0032] In this example, SiO 2 Nanofibers prepared by sol electrospinning as the main material of inorganic flame-resistant paper, TiO 2 As a paper filler, the present invention is further illustrated by examples, but the scope of protection of this patent should not be limited by this. All other inorganic glass precursor sols that can be used for spinning and can be treated by subsequent soaking-drying-compacting-heat treatment Silicate electrospun fiber nonwoven membranes for filling materials such as SiO 2 , CaO, Al 2 o 3 , ZrO 2 etc. and their mixtures are suitable for the inorganic flame-resistant paper disclosed in the present invention.
[0033] The preparation process of the inorganic flame-resistant paper of the present embodiment is as follows:
[0034] Step 1. With ethyl orthosilicate (TEOS), absolute ethanol (EtOH), water (H 2 O), acids (including hydrochloric acid (HCl), nitric acid (HNO 3 ), sulfuric acid (H 2 SO 4 ), acetic acid) as raw materials, and sy...
Embodiment 2-25
[0048] The silicate electrospun nanofiber that the present invention relates to, its composition is SiO 2 As the main body, Al can also be added 2 o 3 , ZrO 2 and other components to improve the mechanical and thermal properties of the fiber. Illustrate below through embodiment 2-25. The main feature of embodiment 2-25 is to adjust the molar ratio of each added raw material in the spinning sol, as shown in table 2:
[0049] The mass ratio of each raw material in the spinning sol of the embodiment 2-25 of table 2
[0050]
[0051]
[0052] The operation steps are as follows:
[0053] Step 1. Use tetraethyl orthosilicate (TEOS), aluminum nitrate pentahydrate (Al(NO 3 ) 3 ·5H 2 O), zirconium nitrate pentahydrate (Zr(NO 3 ) 2 ·5H 2 O), ethanol (EtOH), water (H 2 O), hydrochloric acid (HCl), as raw materials, synthesize spinnable sol by sol-gel technology. The above raw materials were uniformly mixed according to the proportion listed in Table 1, and then a spinn...
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