Preparation method of fractured carbonate rock core

A carbonate and core technology, applied in the field of oil and gas field development, can solve the problems of uncontrollable fracture width, inability to simulate propped fractures, low success rate, etc.

Inactive Publication Date: 2016-02-03
SOUTHWEST PETROLEUM UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Using the method of mechanical destruction to create fractures, the success rate is low, and the formed fractures are relatively random, which cannot be described by exact parameters; although cutting fractures do not have this defect, the core of the cutting part will be missing, and the original shape cannot be maintained , so the core needs to be filled, but the filler used cannot be exactly the same as the matrix core; moreover, the current artificial cemented core is mostly made of quartz sand, and the production method of carbonate rock artificial core is even rarer. And there are certain deficiencies, such as the fractured carbonate core obtained by making carbonate rock slabs, slotting, and drilling cores still has the disadvantage of cutting and creating fractures, and the fractured carbon core obtained by model pressing and anhydrous ethanol washing Although salt core overcomes the defect of cutting and creating fractures, it cannot control the fracture width and cannot simulate propped fractures

Method used

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  • Preparation method of fractured carbonate rock core
  • Preparation method of fractured carbonate rock core
  • Preparation method of fractured carbonate rock core

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0031] Carbonate powder, inorganic glue, and soluble organic gel are mixed evenly according to the ratio of 6.5:2:1.5, and the mixture is put into two semi-cylindrical molds and laid according to the requirements, and the temperature is kept at 45°C for 10 minutes, and the two semi-cylindrical molds are assembled into a cylinder placed on the pressurizing device of the core preparation device, under the condition of 35-40 °C, 10 MPa positive pressure for 20 minutes, and then removed after 10 minutes of back pressure, placed for 3-5 hours, dried at 40 °C, and the irregular end surface was cut off. Soak in 50°C distilled water for 20 minutes in a water bath, and then replace it with 50°C distilled water until the outflowing distilled water is clear, then the required core is obtained. The results are shown in the attached figure 1 shown.

Embodiment 2

[0034] Carbonate powder, inorganic glue, and soluble organic glue are mixed evenly according to 6:2:2, and the mixture is put into two semi-cylindrical molds and laid according to the requirements, and the temperature is kept at 45°C for 10 minutes, and the two semi-cylindrical molds are assembled into a cylindrical shape , placed on the pressurizing device of the core preparation device, under the condition of 35-40°C, 10MPa positive pressure for 20min, and back pressure for 10min, then take it off, place it for 3-5h, dry it at 40°C, cut off the irregular end face, and put it in a water bath Soak the pot with 50°C distilled water for 20 minutes, and then replace it with 50°C distilled water until the outflowing distilled water is clear, then the required core is obtained. The results are shown in the attached figure 2 shown.

[0035] This embodiment and figure 2 It shows that after increasing the proportion of soluble organic gel, the porosity of the core obtained increase...

Embodiment 3

[0037] Carbonate powder, inorganic glue, and soluble organic gel are mixed evenly according to the ratio of 6:2:2, and the mixture is filled into two semi-cylindrical molds and paved as required, and evenly spread on the surface of the substrate laid on one of the semi-cylindrical moulds. Place the selected proppant, pave it with soluble organic gel between the proppants, keep the temperature at 45°C for 10 minutes to make the raw materials in the two semi-cylindrical molds preliminarily cement and form, then assemble the two semi-cylindrical molds into a cylindrical shape, and place them on On the pressurizing device of the core preparation device, under the condition of 35-40°C, press 10MPa positive pressure for 20 minutes, take it off after 10 minutes of back pressure, place it for 3-5 hours, dry it at 40°C, cut off the irregular end face, and put it in a water bath Soak in distilled water at 50°C for 20 minutes, and then replace it with distilled water at 50°C until the out...

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Abstract

The invention provides a preparation method of a fractured carbonate rock core. The method includes: mixing evenly carbonate, an inorganic glue and a soluble organic gel powder, laying the mixture on two semicircular cylinder moulds; laying a proppant of a certain particle size on the surface of one of the semicircular cylinder mixture according to the needs; filling soluble organic gel prepared in advance between the proppant; keeping the two semicircular cylinders containing the materials at a constant temperature in a constant temperature box, and preliminarily molding the materials in the semicircular cylinders; and then assembling the two semicircular cylinders into a cylinder; placing the cylinder in a pressurizing device of a core preparation device for pressing, then soaking in distilled water for 20min, taking out, and displacing the soluble organic gel with distilled water to obtain the support crack rock core with certain width. The preparation method of fractured carbonate rock core not only can prepare the fractured carbonate rock core with proppant support, but also can obtain support fractured carbonate rock cores of different widths through selection of proppant size.

Description

technical field [0001] The invention relates to the technical field of oil and gas field development, in particular to a method for preparing fractured carbonate rock cores. Background technique [0002] In the process of oil and gas field development, many indoor experiments need to use cores, including core flow experiments, core damage experiments, etc. However, the success rate of on-site drilling and coring is low and the cost of coring is high, which greatly increases the cost of experiments, especially for some core experiments on fractured reservoirs, the success rate of coring is lower, and it is difficult to obtain cores with fractures . For this kind of core experiment, especially for the experiment of studying the plugging strength of temporary plugging agent under different fracture widths, it is necessary to obtain cores with different fracture widths, which are almost impossible to obtain on-site drilling and coring, so it is necessary to artificially create ...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N1/28
Inventor 毛金成杨小江李勇明赵金洲
Owner SOUTHWEST PETROLEUM UNIV
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