Preparation method of fractured carbonate rock core
A carbonate and core technology, applied in the field of oil and gas field development, can solve the problems of uncontrollable fracture width, inability to simulate propped fractures, low success rate, etc.
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Embodiment 1
[0031] Carbonate powder, inorganic glue, and soluble organic gel are mixed evenly according to the ratio of 6.5:2:1.5, and the mixture is put into two semi-cylindrical molds and laid according to the requirements, and the temperature is kept at 45°C for 10 minutes, and the two semi-cylindrical molds are assembled into a cylinder placed on the pressurizing device of the core preparation device, under the condition of 35-40 °C, 10 MPa positive pressure for 20 minutes, and then removed after 10 minutes of back pressure, placed for 3-5 hours, dried at 40 °C, and the irregular end surface was cut off. Soak in 50°C distilled water for 20 minutes in a water bath, and then replace it with 50°C distilled water until the outflowing distilled water is clear, then the required core is obtained. The results are shown in the attached figure 1 shown.
Embodiment 2
[0034] Carbonate powder, inorganic glue, and soluble organic glue are mixed evenly according to 6:2:2, and the mixture is put into two semi-cylindrical molds and laid according to the requirements, and the temperature is kept at 45°C for 10 minutes, and the two semi-cylindrical molds are assembled into a cylindrical shape , placed on the pressurizing device of the core preparation device, under the condition of 35-40°C, 10MPa positive pressure for 20min, and back pressure for 10min, then take it off, place it for 3-5h, dry it at 40°C, cut off the irregular end face, and put it in a water bath Soak the pot with 50°C distilled water for 20 minutes, and then replace it with 50°C distilled water until the outflowing distilled water is clear, then the required core is obtained. The results are shown in the attached figure 2 shown.
[0035] This embodiment and figure 2 It shows that after increasing the proportion of soluble organic gel, the porosity of the core obtained increase...
Embodiment 3
[0037] Carbonate powder, inorganic glue, and soluble organic gel are mixed evenly according to the ratio of 6:2:2, and the mixture is filled into two semi-cylindrical molds and paved as required, and evenly spread on the surface of the substrate laid on one of the semi-cylindrical moulds. Place the selected proppant, pave it with soluble organic gel between the proppants, keep the temperature at 45°C for 10 minutes to make the raw materials in the two semi-cylindrical molds preliminarily cement and form, then assemble the two semi-cylindrical molds into a cylindrical shape, and place them on On the pressurizing device of the core preparation device, under the condition of 35-40°C, press 10MPa positive pressure for 20 minutes, take it off after 10 minutes of back pressure, place it for 3-5 hours, dry it at 40°C, cut off the irregular end face, and put it in a water bath Soak in distilled water at 50°C for 20 minutes, and then replace it with distilled water at 50°C until the out...
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