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In vitro cultured calculus bovis aqueous solution and preparation method thereof

A technology for in vitro cultivation of bezoar and aqueous solution, which is applied in the direction of medical formula, medical preparations with non-active ingredients, medical preparations containing active ingredients, etc. It can solve the problems that the active ingredients cannot be fully absorbed and exert their efficacy, and the way of administration is single. , to achieve the effect of improving solubility and promoting absorption

Active Publication Date: 2016-02-24
WUHAN JIANMIN DAPENG PHARMA
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0004] The present invention mainly aims at the problem that the active ingredients in the in vitro cultured bezoar cannot be fully absorbed in the human body and exert their medicinal effects due to the fact that the current in vitro cultured bezoar is taken in pills and powders, and the mode of administration is single, and provides an in vitro cultured bezoar aqueous solution and its Preparation

Method used

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Examples

Experimental program
Comparison scheme
Effect test

example 1

[0016] Grind the bezoar cultivated in vitro into fine powder, pass through a 200-mesh sieve, and set aside; add 5 g of sorbitol and 1 g of essence to 1 L of purified water in sequence, stir, dissolve, and mix well; add 10 g of surfactant poloxamer (PluronicF68) Add it to the above mixed solution; use 1mol / L NaOH to adjust the pH value of the solution to 9.8; then add 10g of sieved in vitro cultured bezoar fine powder to the above mixed solution, and use a homogenizer to stir rapidly for 24h , mix well; centrifuge under the condition of 4000r / min for 15min, take the supernatant, place it at 2-6°C for 5h at low temperature, and then filter; obtain a clear brownish-yellow in vitro cultured bezoar aqueous solution.

example 2

[0018] Grind the bezoar cultivated in vitro into fine powder, pass through a 200-mesh sieve, and set aside; add 8 g of sorbitol and 1.5 g of essence to 1 L of purified water in sequence, stir, dissolve, and mix well; add the surfactant poloxamer (Pluronic F68) Add 15g to the above mixed solution; adjust the pH value of the solution to 9.5 with 1mol / L NaOH; then add 15g of sieved in vitro cultured bezoar fine powder to the above mixed solution, and stir rapidly with a homogenizer 24h, mix well; centrifuge under the condition of 4000r / min for 20min, take the supernatant, put it at 2-6°C for 5h, and then filter to obtain a clear brown yellow in vitro cultured bezoar aqueous solution.

example 3

[0020] Grind the bezoar cultivated in vitro into fine powder, pass through a 200-mesh sieve, and set aside; add 7 g of sorbitol and 1.5 g of essence to 1 L of purified water, stir, dissolve, and mix well; add 8010 g of surfactant Tween to the above-mentioned In the mixed solution; use 0.5 mol / L sodium carbonate to adjust the pH value of the solution to 9; then add 15 g of sieved in vitro cultured bezoar fine powder to the above mixed solution, and use a homogenizer to stir rapidly for 36 hours and mix well Centrifuge at 3000r / min for 20min, take the supernatant, place it at 2-6°C for 6h, and then filter it to obtain a clear brown-yellow in vitro cultured bezoar solution.

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Abstract

The invention provides an in vitro cultured calculus bovis aqueous solution and a preparation method thereof. The calculus bovis aqueous solution is prepared from the following raw materials in mass concentration: 10 to 15g / L of in vitro cultured calculus bovis, a surfactant, 5 to 8g / L of sorbitol and 1 to 1.5g / L of essence; a pH value of the in vitro cultured calculus bovis aqueous solution is 9 to 10. According to the preparation method, the water solubility of the in vitro cultured calculus bovis is improved by the surfactant, the effects of emulsification and stabilization are achieved, so that the effect of solubilization is realized, a clarified in vitro cultured calculus bovis aqueous solution is prepared, and at the same time the absorption of effective components in a human body can be promoted.

Description

technical field [0001] The invention relates to the field of Chinese patent medicines, in particular to an in vitro cultured bezoar aqueous solution and a preparation method thereof. Background technique [0002] Natural bezoar is the dry gallstones of bovine cattle, which are formed in the gallbladder of cattle for several years. Natural bezoar is a precious Chinese herbal medicine, which has the effects of clearing heart, clearing phlegm, resuscitation, cooling liver, calming wind and detoxification. For febrile disease coma, apoplectic phlegm confusion, convulsions and convulsions, epileptic madness, sore throat, aphtha of the mouth and tongue, carbuncle and furuncle. It can be directly applied to patients, and it can also be used as a raw material to manufacture Chinese patent medicines. There are hundreds of Chinese and Western medicines that need natural bezoar as raw materials. Natural bezoar is expensive, which seriously restricts the development of my country's tra...

Claims

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Application Information

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IPC IPC(8): A61K35/413A61K9/08A61K47/34A61K47/22A61K47/26A61K47/14A61K47/20
CPCA61K9/08A61K35/413A61K47/10A61K47/14A61K47/20A61K47/22A61K47/26
Inventor 罗张龙徐冬平李幼鹤
Owner WUHAN JIANMIN DAPENG PHARMA