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Preparation of nano-fiber bundle transistor and application of nano-fiber bundle transistor in ion sensing

A nanofiber and transistor technology, which is applied in the field of electronic information, can solve the problems of low strength, poor flexibility, and inability to realize the application of micro devices, etc., and achieve the effect of simple operation, simple equipment, and large sensing signal

Active Publication Date: 2016-03-09
WUHAN TEXTILE UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The traditional pure polypyrrole flakes have low strength and poor flexibility. In addition, although the conductive non-woven fabric prepared by in-situ polymerization has high strength and high flexibility, it cannot be applied to micro devices.

Method used

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Examples

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preparation example Construction

[0021] A preparation of a nanofiber bundle-based transistor, the preparation method comprising the following steps:

[0022] a. Preparation of the mixed solution of pyrrole monomer and auxiliary agent

[0023] Mix additives with a concentration of 10g / L-500g / L, pyrrole monomers with a concentration of 3g / L-30g / L, and deionized water at a temperature of 80°C to prepare a mixed solution A, wherein the additive is anthracene Quinone-2,7-sulfonic acid sodium salt or anthraquinone-2-sulfonic acid sodium salt.

[0024] b. Preparation of the mixed solution of oxidizing agent and initiator

[0025] Mix an oxidizing agent with a concentration of 5g / L-100g / L and 5-sulfosalicylic acid with a concentration of 30g / L-450g / L and deionized water at room temperature to prepare a mixed solution B, wherein the oxidizing agent is 9- Hydrated ferric nitrate or ferric chloride or ammonium persulfate.

[0026] c. Preparation of nanofiber bundle-based transistor electrolyte

[0027] Mix PVA with ...

Embodiment 1

[0036] a. Preparation of the mixed solution of pyrrole monomer and auxiliary agent

[0037] Mix the auxiliary agent with a concentration of 10g / L, the pyrrole monomer with a concentration of 3g / L and deionized water at a temperature of 80°C to prepare a mixed solution A, wherein the auxiliary agent is anthraquinone-2,7-sulfonic acid sodium salt.

[0038] b. Preparation of the mixed solution of oxidizing agent and initiator

[0039] Mix an oxidant with a concentration of 5 g / L, 5-sulfosalicylic acid with a concentration of 30 g / L, and deionized water at room temperature to form a mixed solution B, wherein the oxidant is ferric nitrate 9-hydrate.

[0040] c. Preparation of nanofiber bundle-based transistor electrolyte

[0041] Mix PVA with a concentration of 80g / L and phosphoric acid with a concentration of 100g / L and deionized water at 80°C to form a mixed solution C.

[0042] d. Pyrrole in situ polymerization of nanofiber bundles

[0043] At 5°C, put the PVA-co-PE nanofibe...

Embodiment 2

[0049] a. Preparation of the mixed solution of pyrrole monomer and auxiliary agent

[0050] Mix the auxiliary agent with a concentration of 250g / L, the pyrrole monomer with a concentration of 15g / L and deionized water at a temperature of 80°C to prepare a mixed solution A, wherein the auxiliary agent is anthraquinone-2,7-sulfonic acid sodium salt.

[0051] b. Preparation of the mixed solution of oxidizing agent and initiator

[0052] Mix an oxidant with a concentration of 50 g / L, 5-sulfosalicylic acid with a concentration of 200 g / L, and deionized water at room temperature to form a mixed solution B, wherein the oxidant is ferric nitrate 9-hydrate.

[0053] c. Preparation of nanofiber bundle-based transistor electrolyte

[0054] Mix PVA with a concentration of 100g / L and phosphoric acid with a concentration of 120g / L and deionized water at 80°C to form a mixed solution C;

[0055] d. Pyrrole in situ polymerization of nanofiber bundles

[0056] At 5°C, the PVA- co -Put the...

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PUM

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Abstract

The invention relates to preparation of a nano-fiber bundle transistor and application of the nano-fiber bundle transistor in ion sensing. The high-performance nano-fiber bundle transistor is prepared by polymerizing pyrrole monomers on a nano-fiber bundle in situ, and the nano-fiber bundle transistor is applied in an ion concentration sensor. Polypyrrole has good chemical and thermodynamic stability, biocompatibility and electric conduction performance, nano-fiber has stitchability, high specific surface area and high surface activity, and can be used for preparation and application of the high-performance transistor. The preparation method is simple in process, gentle in reaction condition, low in production cost, free of pollution and suitable for preparing the nano-fiber bundle transistor on a large scale, and has great application potential in electronic microcircuits.

Description

technical field [0001] The invention relates to the preparation of a nanofiber bundle-based transistor and its application in ion sensors, belonging to the technical field of electronic information. Background technique [0002] Nanofiber refers to a linear material with a diameter of nanoscale and a large length. Due to its small size effect, surface effect and high adsorption, it has a wide range of uses. For example, nanofibers are implanted on the surface of a fabric to form a layer of Stable gas film, made of amphiphobic interface fabric, which can not only waterproof, but also oil-proof and anti-fouling; advanced protective clothing made of nanofibers, the fabric is porous and has a membrane, which not only allows air to pass through, but also has It is breathable, can also block wind and filter fine particles, has barrier properties to aerosols, and can prevent biological and chemical weapons and toxic substances. In addition, nanofibers can also be used for purifica...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): G01N27/414
CPCG01N27/4146
Inventor 王跃丹王栋周舟卿星钟卫兵吴永智刘琼珍
Owner WUHAN TEXTILE UNIV
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