Preparation method of forward osmosis membrane modified with oxidized graphene
A graphene modification, forward osmosis membrane technology, applied in chemical instruments and methods, semi-permeable membrane separation, membrane technology and other directions, can solve the problems of large internal concentration polarization, unstable flux, low strength, etc. Simple process, simple film forming process, easy to achieve effect
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[0050] Example 1.
[0051] Disperse 0.1% graphene oxide uniformly in 35% DMAC for 1 hour, then add 35% 1,4-dioxane and 13% acetone, additives 3.8% methanol, and 3.1% lactic acid into the dispersion at once , And finally add 10% high molecular polymer cellulose triacetate (CTA). Stir it in a 50°C constant temperature water bath until it is completely dissolved, and place it in a 50°C vacuum drying oven (vacuum degree of 0.08MPa) and let it stand to degas for more than 12 hours. Then, in an environment with a temperature of 20°C and a relative humidity of 70%, the film was scraped by a manual scraper using a phase inversion method. The supporting layer was a 150 mesh polyester screen. After the scraped film was volatilized in the air for 30 seconds, put it in In a coagulation bath of deionized water at 20°C, coagulate for 4 hours. Separate the membrane from the glass plate, and put the new membrane into pure water to fully soak for 48 hours to obtain a supported graphene oxide fl...
Example Embodiment
[0053] Example 2
[0054] Disperse 0.1% graphene oxide uniformly in 32% DMAC for 1 hour, then add 32% 1,4-dioxane, 12.4% acetone, additives 6% methanol, and 4.5% lactic acid to the dispersion at once , And finally add 13% polymer cellulose acetate (CA). Stir it in a 60°C constant temperature water bath until it is completely dissolved, and put it in a 60°C vacuum drying oven (vacuum degree of 0.08MPa) and let it stand for 12h or more to degas. Then, in an environment with a temperature of 20°C and a relative humidity of 70%, the film was scraped by a manual scraper using a phase inversion method. The supporting layer was a 150 mesh polyester screen. After the scraped film was volatilized in the air for 30 seconds, put it in In a coagulation bath of deionized water at 20°C, coagulate for 4 hours. Separate the membrane from the glass plate, and put the new membrane into pure water to fully soak for 48 hours to obtain a supported graphene oxide flat plate forward osmosis membrane....
Example Embodiment
[0056] Example 3
[0057] Disperse 0.1% graphene oxide uniformly in 32% DMAC for 1 hour, then add 32% 1,4-dioxane, 12.4% acetone, additives 6% methanol, and 4.5% lactic acid to the dispersion at once Finally, add 6.5% of the high molecular polymer cellulose triacetate (CTA) and 6.5% of the high molecular polymer cellulose acetate (CA), stir in a constant temperature water bath at 60°C until it is completely dissolved, and put it in 60°C In the vacuum drying oven (vacuum degree of 0.08MPa), let it stand for more than 12h to degas. Then, in an environment with a temperature of 20°C and a relative humidity of 70%, the film was scraped by a manual scraper using a phase inversion method. The support layer was a 250 mesh polyester screen. After the scraped film was volatilized in the air for 30 seconds, put it in In a coagulation bath of deionized water at 20°C, coagulate for 4 hours. Separate the membrane from the glass plate, and put the new membrane into pure water to fully soak f...
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