A preparation method of mesoporous perovskite oxide/silicon dioxide and its application method in water treatment
A perovskite type, silicon dioxide technology, applied in the direction of oxidized water/sewage treatment, metal/metal oxide/metal hydroxide catalyst, chemical instruments and methods, etc., can solve the problems of poor treatment effect and achieve high efficiency The effect of removal
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[0014] Specific implementation mode 1: perovskite oxide / SiO 2The preparation method of mesoporous material is: (1) Preparation of CTAB solution, weigh 1.0g ~ 4.0g cetyltrimethylammonium bromide (CTAB), add 60 ~ 120mL deionized water as solvent, ultrasonic 30 ~ 60min to its complete dissolution; (2) preparation of silicon source and active metal solution, add 2.0~10.0mmol lanthanum nitrate, 2.0~10.0mmol cobalt nitrate, 6.0~30.0mmol citric acid (the mol ratio of metal / citric acid=1 / 3), tetraethyl orthosilicate (TEOS) was slowly added dropwise to the solution described in (1) at a molar ratio n(CTAB) / n(TEOS)=0.12, and stirred at room temperature for 24h; (3) to ( 2) Add NaOH with a concentration of 2.0M dropwise to the solution, adjust the pH of the solution to 10.5-11.5 and continue to stir at room temperature for 10-14 hours; (4) Hydrothermal reaction, transfer the solution obtained in step (3) to the stainless steel reactor In the polytetrafluoroethylene lining, hydrothermal...
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