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Pickling equipment and pickling method for rare metal pipes and rare metal alloy pipes

A technology for rare metal and pickling equipment, applied in the field of pickling of rare metal materials, can solve the problems of low acid usage rate, equipment loss, harsh production environment, etc. Effect

Active Publication Date: 2018-05-11
XIAN HAILIAN PETROCHEM TECH
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

The acid usage rate is low, and the plant is filled with acid mist, causing losses to other equipment
The production environment is extremely harsh

Method used

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  • Pickling equipment and pickling method for rare metal pipes and rare metal alloy pipes
  • Pickling equipment and pickling method for rare metal pipes and rare metal alloy pipes
  • Pickling equipment and pickling method for rare metal pipes and rare metal alloy pipes

Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0037] like figure 1 , figure 2 and image 3 As shown, the pickling equipment of the present invention includes an acid storage tank 1, a pressurized tank 2, a confluence tank 5, a diversion tank 6, an acid water collector 7 and a waste acid tank 10, and the acid storage tank 1 and the pressurized tank 2 connection, the pressurized tank 2 is connected with the gas storage tank 3, the two ends of the confluence tank 5 are closed, and one side thereof is connected with the pressurized tank 2, the gas storage tank 3 and the water storage tank 4, and the other side is set There are a plurality of interfaces 5-1 connected to one end of the pipe material 12, the other end of the pipe material 12 goes deep into the diversion groove 6, the bottom end of the diversion groove 6 is provided with an outlet, and the acid water collector 7 is located in the Below the outlet and its bottom are provided with a first passage 7-2 communicating with the acid storage tank 1 and a second passag...

Embodiment 2

[0047] combine Figure 1 to Figure 3 In this embodiment, the method for pickling rare metal pipes and rare metal alloy pipes using the equipment described in Embodiment 1 includes the following steps:

[0048] Step 1. Preparatory work: install one end of a plurality of pipes 12 to be pickled on the interface 5-1, and the other end goes deep into the diversion tank 6, put the acid solution into the acid storage tank 1, and then open the first valve 9 -1 and the second valve 9-2, the acid solution is injected into the pressurized tank 2, then the first valve 9-1 and the second valve 9-2 are closed, the third valve 9-3 is opened, and the acid solution is injected into the pressurized tank 2 Inflate, close the third valve 9-3 after the pressure in the pressurized tank 2 rises to 0.1MPa;

[0049] In this embodiment, the pipe 12 to be pickled is specifically a titanium pipe, the inner diameter of the pipe is 20mm, the length of the pipe is 2000mm, and the number of pipes 12 to be pic...

Embodiment 3

[0055] combine Figure 1 to Figure 3 In this embodiment, the method for pickling rare metal pipes and rare metal alloy pipes using the equipment described in Embodiment 1 includes the following steps:

[0056] Step 1. Preparatory work: install one end of a plurality of pipes 12 to be pickled on the interface 5-1, and the other end goes deep into the diversion tank 6, put the acid solution into the acid storage tank 1, and then open the first valve 9 -1 and the second valve 9-2, the acid solution is injected into the pressurized tank 2, then the first valve 9-1 and the second valve 9-2 are closed, the third valve 9-3 is opened, and the acid solution is injected into the pressurized tank 2 Inflate, close the third valve 9-3 after the pressure in the pressurized tank 2 rises to 0.1MPa;

[0057] In this embodiment, the pipe material 12 to be pickled is specifically a titanium alloy pipe, the inner diameter of the pipe material is 15mm, the length of the pipe material is 1800mm, a...

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Abstract

The invention provides acid pickling equipment for rare metal tubes and rare metal alloy tubes. The acid pickling equipment comprises an acid storage trough, a pressurizing tank, a confluence tank, a diversion trough, an acid water collector and a waste acid trough. The acid storage trough is connected with the pressurizing tank; the pressurizing tank is connected with a gas storage tank; one side of the confluence tank is connected with the pressurizing tank, the gas storage tank and a water storage tank, the other side of the confluence tank is provided with a plurality of connectors connected with the rare metal tubes and the rare metal alloy tubes, and the other ends of the tubes are inserted into the diversion trough; the acid water collector is located under an outlet opening, and a passage is installed at the bottom of the acid water collector; and the passage communicates with the acid storage trough and the waste acid trough. The invention further provides an acid pickling method for the rare metal tubes and the rare metal alloy tubes using the acid pickling equipment. According to the acid pickling equipment and the acid pickling method for the rare metal tubes and the rare metal alloy tubes, acid pickling work can be conducted on the rare metal tubes and the rare metal alloy tubes; almost no acid mist and acid gas suffuse in the working environment; no harm is done to health; acid pickling effect is remarkable; and the recovery rate of acid liquor is high.

Description

technical field [0001] The invention belongs to the technical field of pickling of rare metal materials, and in particular relates to pickling equipment and a pickling method for rare metal pipes and rare metal alloy pipes. Background technique [0002] Pickling is an indispensable process in the processing of nuclear rare metal pipes and rare metal alloy pipes. When the diameter of the pipe is too small, due to the existence of the surface tension of the liquid, it is difficult for the acid to flow on the inner surface of the pipe, and the effect of pickling and decontamination of the pipe cannot be achieved. [0003] In order to solve this problem, the traditional pickling equipment is usually equipped with an open tank with a high position to hold the acid solution, so that the acid solution flows through the inside of the rare metal pipe through the pipeline to achieve the purpose of pickling. This method is suitable for small batches, but not suitable for industrial pr...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C23G3/04C23G1/02
CPCC23G1/02C23G3/04
Inventor 张乃禄孟智彬闫锋
Owner XIAN HAILIAN PETROCHEM TECH