A kind of preparation method of fuel additive
A technology of additives and fuel oil, applied in the direction of fuel additives, fuel, petroleum industry, etc., can solve the problems of polluting the environment, human body, injury, etc., and achieve the effects of less carbon deposition, sufficient combustion, and reduced exhaust emissions
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example 1
[0019] First, select 5 snails with a weight of 30 g, wash them with deionized water for 3 times, smash the shells of the snails after cleaning, peel off the shells, crush the shells with a pulverizer for 10 minutes, collect the crushed objects, and add them to a beaker. Add 100mL of absolute ethanol to the beaker, place it in an ultrasonic oscillator, ultrasonicate at 220W for 30min, then filter, collect the filtrate and filter residue respectively, and set aside; then weigh 5g of polyisobutylene and add it to a three-necked flask with a thermometer and a reflux device , put the flask in an oil bath, heat up to 80°C, then add 1g of maleic anhydride, stir for 30min, then heat up to 160°C, then add 2mL of 1-amino-8-naphthol-3,6-disulfone acid, stirred for 2 hours, after the reaction was completed, added diethylene polyethylamine, adjusted the pH to 7.0, then added 100mL deionized water, stirred for 10 minutes, allowed to stand and separated, collected the organic phase, that is, ...
example 2
[0022]First select 6 snails with a weight of 35g, wash them with deionized water for 4 times, smash the shells of the snails after cleaning, peel off the shells, crush the shells with a pulverizer for 15 minutes, collect the crushed objects, and add them to the beaker. Add 150mL of absolute ethanol to the beaker, place it in an ultrasonic oscillator, ultrasonicate at 230W for 35min, then filter, collect the filtrate and filter residue respectively, and set aside; then weigh 7g of polyisobutylene and add it to a three-necked flask with a thermometer and a reflux device , put the flask in an oil bath, raise the temperature to 85°C, then add 2g of maleic anhydride, stir for 35min, then raise the temperature to 165°C, then add 3mL of 1-amino-8-naphthol-3,6-disulfone acid, stirred for 2.5 hours, and after the reaction was completed, added diethylenepolyethylamine to adjust the pH to 7.0, then added 150 mL of deionized water, stirred for 15 minutes, allowed to stand for layers, and c...
example 3
[0025] First, select 7 snails with a weight of 40 g, wash them with deionized water for 5 times, smash the shells of the snails after cleaning, peel off the shells, crush the shells with a pulverizer for 20 minutes, collect the crushed objects, and add them to the beaker. Add 200mL of absolute ethanol to the beaker, place it in an ultrasonic oscillator, ultrasonicate at 240W for 40min, then filter, collect the filtrate and filter residue respectively, and set aside; then weigh 8g of polyisobutylene and add it to a three-necked flask with a thermometer and a reflux device , put the flask in an oil bath, heat up to 90°C, then add 3g of maleic anhydride, stir for 40min, then heat up to 170°C, then add 4mL of 1-amino-8-naphthol-3,6-disulfone acid, stirred for 3 hours, after the reaction was completed, added diethylenepolyethylamine, adjusted the pH to 7.0, added 200mL of deionized water, stirred for 20min, allowed to stand and separated, and collected the organic phase, that is, po...
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