Method for assisting brazing by carbon nanotube reinforced type three-dimensional middle layer
A carbon nanotube, three-dimensional structure technology, applied in the field of brazing ceramics and metals, can solve the problems of insufficient high temperature performance and large residual stress, and achieve the effects of improving high temperature performance, relieving residual stress and relieving residual stress.
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[0022] Specific embodiment 1: The method for assisted brazing of the intermediate layer of carbon nanotube reinforced three-dimensional structure described in this embodiment is performed according to the following steps:
[0023] 1. Wash the foamed metal with hydrochloric acid, acetone, absolute ethanol and deionized water with a concentration of 1mol / L~3mol / L for 10 minutes, and then dry naturally to obtain the pretreated foamed metal. Add the catalyst to the Obtain anhydrous ethanol solution of the catalyst with a concentration of 0.001mol / L~1mol / L in water ethanol, and immerse the pretreated metal foam in the anhydrous ethanol solution of the catalyst with a concentration of 0.001mol / L~1mol / L , Let it stand for 1h, and then dry naturally to obtain the foamed metal after soaking;
[0024] 2. Place the soaked metal foam in a plasma-enhanced chemical vapor deposition vacuum device, evacuate to a pressure of 20Pa-100Pa or less, pass in hydrogen gas, adjust the hydrogen gas flow rat...
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[0036] Specific embodiment two: this embodiment is different from specific embodiment one in that: the foamed metal in step one is foamed copper or foamed nickel. Others are the same as the first embodiment.
Example Embodiment
[0037] Specific embodiment three: This embodiment is different from one of specific embodiments one or two in that the catalyst in step one is nickel nitrate hexahydrate, iron nitrate, cobalt nitrate, nickel sulfate, iron sulfate or cobalt sulfate. Others are the same as the first or second embodiment.
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