A kind of elastic finishing agent for textile finishing and its preparation method and using method
A technology for finishing agents and textiles, applied in the field of dyeing and finishing auxiliaries, which can solve the problems of inability to mix finishing agents and many textile finishing processes, and achieve the effects of reducing energy consumption, good water resistance, and improving processing efficiency
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Embodiment 1
[0051]Weigh 55g of butyl acrylate, 80g of styrene, 2g of methacryloxyethyltrimethylammonium chloride, 3g of allyl polyoxyethylene methyl ether, 5g of hydroxyethyl methacrylate, cationic emulsifier ( 1831) 0.5g, nonionic emulsifier (EFS-1310) 1g, ammonium persulfate 0.33g, glacial acetic acid 1g and deionized water 140g were added to the first reaction vessel;
[0052] Control the stirring speed at about 2000rpm at room temperature, stir for 30 minutes, and prepare a milky white non-layered pre-emulsion;
[0053] Take by weighing 40g pre-emulsion and add in the second reaction vessel;
[0054] Weigh 0.5g of cationic emulsifier (1831), 1g of nonionic emulsifier (EFS-1310), 0.33g of ammonium persulfate and 200g of deionized water into the second reaction container;
[0055] Continue stirring at a speed of 1800 rpm for 10 minutes at room temperature to prepare a primer;
[0056] Into the second reaction vessel, first pass nitrogen gas into it for about 30 minutes to remove oxyge...
Embodiment 2
[0062] Weigh 56g of butyl acrylate, 70g of styrene, 9g of acrylonitrile, 2g of methacryloxyethyltrimethylammonium chloride, 3g of allyl polyoxyethylene methyl ether, 5g of hydroxyethyl methacrylate, Add 0.5g of cationic emulsifier (1831), 1g of nonionic emulsifier (EFS-1310), 0.33g of ammonium persulfate, 1g of glacial acetic acid and 140g of deionized water into the first reaction vessel;
[0063] Control the stirring speed at about 2200 rpm at normal temperature, and stir for 40 minutes to prepare a milky white non-layered pre-emulsion.
[0064] Take by weighing 40g pre-emulsion and add in the second reaction vessel;
[0065] Weigh 0.5g of cationic emulsifier (1831), 1g of nonionic emulsifier (EFS-1310), 0.33g of ammonium persulfate and 200g of deionized water into the second reaction container;
[0066] Continue stirring at a speed of 2000 rpm for 15 minutes at room temperature to prepare a primer;
[0067] Into the second reaction vessel, first pass nitrogen gas into it ...
Embodiment 3
[0073] Weigh 54g of butyl acrylate, 70g of styrene, 10g of acrylonitrile, 2g of acryloyloxyethyl dimethyl benzyl ammonium chloride, 3g of allyl polyoxyethylene methyl ether, 5g of hydroxyethyl acrylate, and tallow three Methylammonium chloride 0.5g, nonionic emulsifier (AEO-9) 1g, ammonium persulfate 0.33g, glacial acetic acid 1g and deionized water 140g join in the first reaction vessel;
[0074] Control the stirring speed at about 2200rpm at room temperature, and stir for 35 minutes to prepare a milky white non-layered pre-emulsion;
[0075] Take by weighing 40g pre-emulsion and add in the second reaction vessel;
[0076] Weigh 0.5g of tallow trimethylammonium chloride, 1g of nonionic emulsifier (AEO-9), 0.33g of ammonium persulfate and 200g of deionized water into the second reaction container;
[0077] Continue stirring at a speed of 2200 rpm for 20 minutes at room temperature to prepare a primer;
[0078] Into the second reaction vessel, first pass nitrogen gas into it ...
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