A deep-water white oil plate flow oil-based drilling fluid
A drilling fluid and flat plate technology, which is applied in the field of drilling, can solve the problems of large fluctuations and temperature sensitivity of drilling fluid, and achieve the effects of reduced high-pressure water loss, good anti-pollution performance, and excellent anti-pollution performance
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[0032] Based on 100 parts of white oil, the deep-water white oil plate flow oil-based drilling fluid provided by the present invention contains 2-4 parts of flow pattern regulator, preferably 2.5-3.5 parts, more preferably 2.8-3.3 parts. In the present invention, the flow regulator is preferably prepared from raw materials including acrylic acid, phenylacetic acid and maleic anhydride, and the preparation method of the flow regulator preferably includes the following steps:
[0033] Mix acrylic acid and styrene for primary heat treatment to obtain a primary thermal mixture;
[0034] performing a secondary heat treatment on the primary thermal mixture and maleic anhydride to obtain a flow regulator.
[0035] The invention mixes acrylic acid and styrene for primary heat treatment to obtain a primary heat mixture. In the present invention, the temperature of the primary heat treatment is preferably 80-100°C, more preferably 85-95°C, most preferably 90-92°C; the time of the prima...
Embodiment 1
[0047] The main emulsifier is obtained by mixing oleic acid, dimer acid and tall oil fatty acid according to the mass ratio of 20:40:20.
[0048] Heat 20 parts of oleic acid and 25 parts of tall oil fatty acid to 120°C, vacuumize (vacuum degree -0.1MPa) inhale 30 parts of diethanolamine and 25 parts of triethanolamine, keep warm for 2 hours, and then continue to heat up to 360°C (heating time is 2h), heat preservation reaction for 6h, cooling and discharging to obtain co-emulsifier.
[0049] Mix and stir 30 parts of acrylic acid and 40 parts of styrene evenly, heat to 90°C, react for 1 hour, add 30 parts of maleic anhydride, heat to 160°C, keep warm for 3 hours, cool and discharge to obtain the flow regulator.
[0050] 100 parts of 3# white oil, 2 parts of main emulsifier, 1 part of auxiliary emulsifier, 2 parts of flow regulator, 1.0 part of calcium oxide, 1.5 parts of Pengrun organic soil, 3 parts of modified sulfonated Asphalt, 20 parts of 26% calcium chloride aqueous solu...
Embodiment 2
[0052] The main emulsifier is obtained by mixing oleic acid, dimer acid and tall oil fatty acid according to the mass ratio of 20:10:20.
[0053] Heat 15 parts of oleic acid and 20 parts of tall oil fatty acid to 120°C, vacuumize (vacuum degree -0.1MPa) inhale 35 parts of diethanolamine and 30 parts of triethanolamine, keep warm for 2 hours, and then continue to heat up to 360°C (heating time is 2h), heat preservation reaction for 6h, cooling and discharging to obtain co-emulsifier.
[0054] Mix and stir 30 parts of acrylic acid and 40 parts of styrene evenly, heat to 90°C, react for 1 hour, add 35 parts of maleic anhydride, heat to 160°C, keep warm for 3 hours, cool and discharge to obtain the flow regulator.
[0055] 100 parts of 3# white oil, 2 parts of main emulsifier, 1 part of auxiliary emulsifier, 2 parts of flow regulator, 1 part of magnesium oxide, 1.5 parts of Pengrun organic soil, 3 parts of natural asphalt, 20 parts of 26% calcium chloride aqueous solution and 99 ...
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