Preparation method of artificially synthesized fluorphlogopite powder coated with nano metal silver
A technology of fluorophlogopite powder and nano-metal silver is applied in the field of preparation of synthetic fluorophlogopite powder coated with nano-metal silver, and can solve the problems of small coating amount, large impurity content of composite silver powder, heavy texture, etc.
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Embodiment 1
[0060] In the present embodiment, the preparation method of nano-metallic silver-coated artificially synthesized fluorine phlogopite powder comprises the following steps:
[0061] (1) Pretreatment of artificially synthesized fluorphlogopite powder
[0062] (1-1) Coarsening
[0063] (1-1-1) Take 100 parts by weight of artificially synthesized fluorophlogopite powder (according to dry weight), add it to 400 parts by weight of hydrochloric acid with a concentration of 6mol / L, disperse for 30 minutes, and then let it stand for 1 hour to remove the upper layer Clear liquid, keep the sediment in the lower layer;
[0064] (1-1-2) Washing and dehydrating the precipitate obtained in step (1-1-1) with water to obtain roughened artificially synthesized fluorophlogopite powder;
[0065] In this step (1-1-2), the following method is used to wash and dehydrate the sediment: add 400 parts by weight of deionized water to the sediment and stir, and then use a plate and frame filter press to ...
Embodiment 2
[0083] In the present embodiment, the preparation method of nano-metallic silver-coated artificially synthesized fluorine phlogopite powder comprises the following steps:
[0084] (1) Pretreatment of artificially synthesized fluorphlogopite powder
[0085] (1-1) Coarsening
[0086] (1-1-1) Take 100 parts by weight of artificially synthesized fluorophlogopite mica powder (according to dry weight), add it to 480 parts by weight of hydrochloric acid with a concentration of 6mol / L, disperse for 25 minutes, and then let stand for 0.8 hours to remove the upper layer Clear liquid, keep the sediment in the lower layer;
[0087] (1-1-2) Washing and dehydrating the precipitate obtained in step (1-1-1) with water to obtain roughened artificially synthesized fluorophlogopite powder;
[0088] In this step (1-1-2), the following method is used to wash and dehydrate the precipitate: add 420 parts by weight of deionized water to the precipitate and stir it, and then use a plate and frame fi...
Embodiment 3
[0106] In the present embodiment, the preparation method of nano-metallic silver-coated artificially synthesized fluorine phlogopite powder comprises the following steps:
[0107] (1) Pretreatment of artificially synthesized fluorphlogopite powder
[0108] (1-1) Coarsening
[0109] (1-1-1) Take 100 parts by weight of artificially synthesized fluorphlogopite mica powder (according to dry weight), add it to 320 parts by weight of hydrochloric acid with a concentration of 6mol / L, disperse for 35 minutes, and then let it stand for 1.2 hours to remove the upper layer Clear liquid, keep the sediment in the lower layer;
[0110] (1-1-2) Washing and dehydrating the precipitate obtained in step (1-1-1) with water to obtain roughened artificially synthesized fluorophlogopite powder;
[0111] In this step (1-1-2), the following method is used to wash and dehydrate the precipitate: add 350 parts by weight of deionized water to the precipitate and stir it, and then use a plate and frame ...
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