A kind of extraction process of natural β-carotene
A technology of carotene and extraction process, applied in the direction of organic chemistry, can solve the problems of less research and utilization, immeasurable industrial value, etc., and achieve the effect of broad market prospects
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Embodiment 1
[0026] A process for extracting natural beta-carotene, comprising the steps of:
[0027] (1) Cleaning: clean the collected leaves of the Fagaceae, remove the soil on the surface of the leaves, and remove impurities;
[0028] (2) wall-breaking treatment: the leaves of the Fagaceae plant after step (1) is cleaned and removed are subjected to wall-breaking treatment;
[0029] (3) Extraction: adding an organic solvent to the mixture obtained in step (2) for reflux extraction or ultrasonic extraction;
[0030] (4) centrifugation: the product of step (3) is centrifuged, the upper layer is an orange supernatant, and the lower layer is a filter residue;
[0031] (5) Evaporation: put the orange supernatant obtained in step (4) into an evaporator, and add ethanol to the evaporator to evaporate to obtain the crude product of β-carotene;
[0032] (6) Purification: add water, ethanol, and lye to the crude product of beta-carotene gained in step (5), stir, then put into an evaporator to e...
Embodiment 2
[0040] A process for extracting natural beta-carotene, comprising the steps of:
[0041] (1) Cleaning: clean the chestnut leaves collected, remove the soil on the surface of the leaves, and remove impurities;
[0042] (2) wall-breaking treatment: the leaves of the Fagaceae plant after step (1) is cleaned and removed are subjected to wall-breaking treatment;
[0043] (3) Extraction: adding an organic solvent to the mixture obtained in step (2) for reflux extraction or ultrasonic extraction;
[0044] (4) centrifugation: the product of step (3) is centrifuged, the upper layer is an orange supernatant, and the lower layer is a filter residue;
[0045](5) Evaporation: put the orange supernatant obtained in step (4) into an evaporator, and add ethanol to the evaporator to evaporate to obtain the crude product of β-carotene;
[0046] (6) Purification: add water, ethanol, and lye to the crude product of beta-carotene gained in step (5), stir, then put into an evaporator to evaporate...
Embodiment 3
[0053] A process for extracting natural beta-carotene, comprising the steps of:
[0054] (1) Cleaning: cleaning the collected Chestnut leaves, removing the soil on the surface of the leaves, and removing impurities;
[0055] (2) wall-breaking treatment: the leaves of the Fagaceae plant after step (1) is cleaned and removed are subjected to wall-breaking treatment;
[0056] (3) Extraction: adding an organic solvent to the mixture obtained in step (2) for reflux extraction or ultrasonic extraction;
[0057] (4) centrifugation: the product of step (3) is centrifuged, the upper layer is an orange supernatant, and the lower layer is a filter residue;
[0058] (5) Evaporation: put the orange supernatant obtained in step (4) into an evaporator, and add ethanol to the evaporator to evaporate to obtain the crude product of β-carotene;
[0059] (6) Purification: add water, ethanol, and lye to the crude product of beta-carotene gained in step (5), stir, then put into an evaporator to e...
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