Method for measuring migration quantity of benzene series in food processing electric appliance on basis of dynamic headspace
A technology of dynamic headspace and food processing, which is applied in the direction of instruments, measuring devices, scientific instruments, etc., to achieve the effect of high sensitivity and simple operation
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[0024] 1. Instruments and reagents
[0025] Agilent 6890-5975 Gas Chromatograph-Mass Spectrometer (Agilent, USA), Dynamic Headspace Instrument (DANI, Italy).
[0026] Benzene, p-xylene (Beijing Bailingwei Technology Co., Ltd., purity ≥ 99.0%), ethylbenzene, m-xylene, o-xylene, styrene (Shanghai Macklin Biochemical Technology Co., Ltd., purity ≥ 99%), toluene (Korea Duksan purechemicals, purity ≥ 99.9%), sodium chloride (Xilong Chemical, analytically pure), absolute ethanol (Beijing Chemical Plant, analytically pure), and experimental water was ultrapure water prepared by Milli-Q.
[0027] 2. Solution preparation
[0028] Standard solution: Weigh 20 mg of each standard product, dissolve it in ethanol and dilute it in a 100 mL volumetric flask to prepare a 200 mg / L single-standard stock solution; accurately draw 1 mL of each single-standard stock solution, and dilute it in a 100 mL volumetric flask with ethanol , prepared into 2mg / L mixed standard stock solution. Then diluted...
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