Peptide compounds with antibacterial and anti-inflammatory activities
A technology of peptide compounds and drugs, applied in anti-inflammatory agents, antibacterial drugs, local antibacterial agents, etc., can solve problems such as high production costs, high difficulty in synthesis and purification, and limited application of LL-37
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Embodiment 1
[0032] 1. Experimental method
[0033] 1.1 Polypeptide synthesis
[0034]The standard Fmoc solid-phase synthesis method 1 was used for peptide synthesis, Rink Amide MHBA resin was selected to synthesize peptides in ABI 433A peptide synthesizer, and the purified peptide (85.0%-90.0%) was completely dissolved in sterile deionized water at a concentration of 5mg / mL , and stored in a freezer at 4°C; the amino acid of the Fmoc protecting group needs an 8-fold excess; HBTU and HOBt are in an 8-fold excess, and DIEA is in a 16-fold excess. DMF is used as a solvent to dissolve HBTU, HOBt, and DIEA. After the last amino acid is condensed completely, a 10-fold excess fatty acid reaction is connected to the resin, and the reaction conditions are standard amino acid coupling reaction conditions. The synthesized lipopeptide is cleaved from the resin with the M reagent, the M reagent is trifluoroacetic acid: ethanedithiol: sulfide anisole: water = 100:1:2:2, the reaction time is 3h, and th...
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