Preparation method and use of carbon-based composite material
A technology of carbon-based composite materials and electrode materials, which is applied in the manufacture of hybrid/electric double layer capacitors and electrodes of hybrid capacitors. Convenient preparation method, easy diffusion and transmission effect
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Embodiment 1
[0062] 1) Preparation of HKUST-1 metal organic framework thin film
[0063] Weigh copper acetate and trimesic acid, dissolve them in pure ethanol solution, and prepare 500ml of solutions with concentrations of 1mmol / L and 0.4mmol / L respectively.
[0064] The prepared solutions are respectively connected to the circulation pump device to provide the reaction raw materials, and each pump correspondingly draws a solution. Then, the cotton cloth modified with hydroxyl groups was used as the growth substrate, and the cotton cloth was fixed in the reaction pool. Finally, set the time for extracting the solution, soaking time and reaction time, and start the cycle after the setting is completed.
[0065] Wherein, the immersion amount of copper acetate solution is advisable to have not crossed cotton cloth, and immersion time is 15 minutes, and standing reaction time is 3 minutes after immersion, and soaks 1 minute with pure ethanol after reaction to remove residual reaction raw mate...
Embodiment 2
[0073] 1) Preparation of ZIF-8 metal-organic framework films
[0074] Weigh zinc acetate and dimethylimidazole, dissolve them in pure ethanol solution, and prepare 500ml of solutions with concentrations of 1mmol / L and 0.4mmol / L respectively.
[0075] The prepared solutions are respectively connected to the circulation pump device to provide the reaction raw materials, and each pump correspondingly draws a solution. Then, the cotton cloth modified with hydroxyl groups was used as the growth substrate, and the cotton cloth was fixed in the reaction pool. Finally, set the time for extracting the solution, soaking time and reaction time, and start the cycle after the setting is completed.
[0076] Wherein, the immersion amount of zinc acetate solution is advisable to have not crossed cotton cloth, immersion time is 15 minutes, after immersion standstill reaction time is 3 minutes, after reaction, soak 1 minute with pure ethanol to remove residual reaction raw material. Afterward...
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