Patents
Literature
Patsnap Copilot is an intelligent assistant for R&D personnel, combined with Patent DNA, to facilitate innovative research.
Patsnap Copilot

355results about How to "Synthesis speed" patented technology

Method for reducing and preparing functionalized nano-silver based on polyphenol

The invention discloses a novel method for reducing and preparing functionalized nano-silver based on polyphenol. The preparation process is as follows: 1), stock solutions of all reaction liquids are prepared, and the stock solutions comprise a silver-bearing predecessor stock solution, a polyphenol compound stock solution and an alkaline stock solution; 2), a polyphenol compound solution is prepared: a certain amount of the polyphenol compound stock solution is taken and added into ultrapure water, and the stock solution and the ultrapure water are mixed uniformly; 3), the pH value and the temperature of the polyphenol compound solution are adjusted: a proper amount of the alkaline stock solution is taken and added into the polyphenol compound solution prepared in the step 2), the pH value of the mixed solution is adjusted, the mixed solution is placed and kept out of the sun, and the temperature of the mixed solution is adjusted; and 4), a nano-silver solution is generated: a certain amount of the silver-bearing predecessor stock solution is added into the mixed solution with adjusted pH value and temperature in the step 3) and is kept out of the sun, and reaction is performed for a certain time. The operation method is simple, the synthesis speed is high, the cost is low, the biocompatibility is high, the method is pollution-free, the sizes of the synthesized nano-silver particles are small, the monodispersity is good, and the nano-silver also has the performance of a polyphenol compound.
Owner:SOUTHEAST UNIV

Method for preparing rare-earth vanadate LaVO4:Eu red fluorescent powder

The invention discloses a method for preparing rare-earth vanadate LaVO4:Eu red fluorescent powder, which comprises the following steps: weighing La2O3 and Eu2O3 according to molar ratio; dissolving two oxides with concentrated nitric acid, and diluting the two oxides with deioniezed water; weighing NH4VO3 of which the mole number is two times that of rare-earth oxide to be prepared into dilute solution, and adding the dilute solution into rare-earth solution to obtain yellow clear solution; adding citric acid of which the mole number is 0.75 time that of rare-earth atoms and taken as a complexing agent into the yellow clear solution; adjusting the pH value of the mixed solution to be 5 to 7 with nitric acid and ammonia water; pouring the obtained emulsion into a polytetrafluoroethylene reaction kettle after the mixed solution is stirred, placing the reaction kettle into a microwave oven, and performing microwave irradiation for 8 to 10 minutes; and removing supernatant liquid after performing high speed centrifugation on the obtained suspension liquid, and washing and drying sediment to obtain the red fluorescent powder LaVO4:Eu. The method has the advantages of simple and convenient operation and quick synthesis. The obtained powder has the characteristics of high purity, high crystallinity, uniform particle size, and stable luminescence.
Owner:ZHEJIANG SCI-TECH UNIV

Intelligent group photo taking method and device, electronic equipment and storage medium

The invention relates to the technical field of image processing, and discloses an intelligent group photo taking method and device, electronic equipment and a storage medium, and the method comprisesthe steps: responding to a group photo taking instruction inputted through a photographing operation interface, obtaining a photographed first image, and obtaining reserved region information specified for a to-be-group-photo target in the first image through the photographing operation interface; in response to a sending instruction input through the shooting operation interface, sending a groupphoto request to a background server, the group photo request comprising the first image and reserved area information; and receiving a group photo image sent by the background server, wherein the group photo image is obtained by fusing a target image corresponding to the target to be subjected to group photo taking into the first image by the background server according to the reserved area information, and the target image is extracted from a second image containing the target to be subjected to group photo taking. According to the technical scheme provided by the embodiment of the invention, the operation is simple, the image synthesis speed is high, and the group photo image fusion effect is good.
Owner:TENCENT TECH (SHENZHEN) CO LTD

System for preparing indium phosphide crystals by utilizing indium-phosphorus mixture

The invention discloses a system for preparing indium phosphide crystals by using an indium-phosphorus mixture. The invention belongs to the technical field of semiconductors. The system comprises a vacuum system, an inflation and deflation system, a temperature and pressure control system, an electrical control system, a cooling circulation system, a weighing system and a furnace body, wherein acrucible rod rotary lifting mechanism and a seed crystal rod lifting mechanism are arranged on the furnace body; the system is characterized in that the furnace body is divided into a synthetic growthchamber, a feeding chamber and a charging chamber, the charging chamber and the feeding chamber are separated by an inserting plate, a turnover feeder is arranged in the charging chamber, a feeding pipe is arranged in the feeding chamber, one end of the feeding pipe is in butt joint with the turnover feeder, and the other end of the feeding pipe extends into a crucible in the synthetic growth chamber to form an indium-phosphorus mixed ball feeding structure; wherein the crucible is positioned on a crucible rod, and a seed crystal rod lifting mechanism is arranged on a top cover of the synthetic growth chamber. Indium-phosphorus mixed balls can be rapidly put into the crucible covered with liquid boron oxide, indium phosphide crystals are formed through in-situ pulling after synthesis, thesynthesis speed is higher, and industrial production is facilitated.
Owner:THE 13TH RES INST OF CHINA ELECTRONICS TECH GRP CORP

Industrial fermentation method of riboflavin

ActiveCN102154426AIncreased industrial fermentation unitsImproving the process conditions of fed-batch fermentationFermentationGLUCOSE LIQUIDCulture mediums
The invention discloses an industrial fermentation method of riboflavin, which comprises the following steps of: filling a seed culture medium into a 10m<3> seed tank, and performing oxic cultivation; and filling a fermentation medium into a 200m<3> fermentation tank for fermentation, mechanically stirring, adding sterilization starch glucose liquid, stopping fermenting till that the glucose is completely consumed or the dissolved oxygen is raised to be 60%, and extracting the riboflavin from the fermentation liquid. After the industrial fermentation method is used, the conventional riboflavin material-supplementing fermentation technology is changed, the low-concentration raw material cultivating bacteria is adopted, the material is quantificationally supplemented according to the changeof the dissolved oxygen of the fermentation solution, the excessive multiplication of the thallus can be effectively controlled, the deviation of the optimum control temperature caused by the excessive supersession can be avoided, the defects of the insufficient ventilation and oxygen supply can be remitted, and the thallus vigor can be kept, so that the indusial fermentation unit of the riboflavin is improved by more than 18g/L, and the yield is increased by 20% compared with the common fermentation.
Owner:GUANGJI PHARMA MENGZHOU

Fisheye panoramic image synthesis processing method and device

The embodiment of the invention discloses a fisheye panoramic image synthesis processing method and device. The fisheye panoramic image synthesis processing method comprises the steps of acquiring first test fisheye images of a chessboard target, processing the first test fisheye images according to a Zhengyou Zhang calibration algorithm to acquire intrinsic parameters of a fisheye camera; acquiring second test fisheye images of an annular target, and acquiring extrinsic parameters of the fisheye camera according to an iterative closest point algorithm; acquiring fisheye images to be synthesized, acquiring a corresponding relation between pixel coordinates of the fisheye images to be synthesized and pixel coordinates of fisheye image nonstandard Thoby expanded image according to the intrinsic parameters and the extrinsic parameters; processing the fisheye images to be synthesized according to the corresponding relation to acquire a synthesized panoramic image. The corresponding relation between the pixel coordinates of the fisheye images to be synthesized and pixel coordinates of the panoramic image can be acquired through acquiring the intrinsic parameters and the extrinsic parameters of the fisheye camera, thereby being convenient for processing according to the corresponding relation to acquire the synthesized panoramic image. The original images are photographed simply, the image synthesizing process is high in automation degree, and real-time image synthesis can be performed.
Owner:北京的卢深视科技有限公司

Method for preparing silicon carbide ceramic

The invention discloses a method for preparing carborundum ceramic, which comprises the following steps: mixing bamboo charcoal with silicon powder after crushing and grinding bamboo charcoal by solid phase sintering, according to the mass ratio of 1 to 3, and evenly mixing the mixture of silicon and charcoal with phenolic resin according to the weight volume ratio of 1 to 1; preheating the mixture at the temperature of 140 DEG C for molding; under the state of vacuum or Ar gas atmosphere, increasing the temperature to the set final sintering temperature for high-temperature sintering; maintaining the temperature for 30 minutes, and cooling the mixture to produce the SiC ceramic material. In the method, carbide materials can be produced by an organic texture of bamboo materials through high-temperature sintering, the bamboo materials are charred under anaerobic condition to produce a charcoal frame with a bamboo pore structure, and the charcoal frame can be used as a biological template for ceramic phase filtering and reacting. The ceramic obtained through filtering and sintering reactions of metal or inorganic non-metal substances not only has a fine structure of bamboo, but also increases the reacting area, improves the resultant velocity, and has advantages superior to the prior ceramic preparation method.
Owner:INST OF WOOD INDUDTRY CHINESE ACAD OF FORESTRY

Method for quickly acclimatizing active sludge mixed flora to prepare polyhydroxyalkanoate (PHA) by using aerobic dynamic drainage method

The invention discloses a method for quickly acclimatizing active sludge mixed flora to prepare polyhydroxyalkanoate (PHA) by using an aerobic dynamic drainage method and relates to a method for preparing the PHA. The invention solves the problems that the acclimatization time for synthesizing PHA through active sludge mixed flora is long, a reactor works unstably and the synthesized PHA is low in content in the prior art. The method comprises the following steps: 1, active sludge is put into a sequencing batch reactor (SBR); 2, 6-12 hours are taken as a cycle of operation, in the cycle of operation, two-time water introduction, precipitation and drainage are carried out, the drainage rate is 1:1, during the first water introduction, a carbon source and various nutrients are introduced, and during the second water introduction, only the supplement of nitrogen nutrient is carried out; 3, 2-4 cycles are operated every day, the sludge detention time is 1-10 days and sludge-water mixed liquid is collected; 4, batch experiments are carried out, half supernatant is discharged, equivalent carbon source is supplemented, aeration, precipitation and drainage are carried out, and the process is repeated for 6 to 8 times. The invention belongs to the field of biodegradable plastic synthesis.
Owner:HARBIN INST OF TECH

Process for liquid-phase synthesis of diindium triselenide in double temperature zone vacuum tight tube

InactiveCN102275880APrevent tube explosionPrevent split tube phenomenonBinary selenium/tellurium compoundsIndiumHeating furnace
A liquid phase synthesis process of diindium triselenide double-temperature zone vacuum tight tube is characterized by comprising the following steps: 5N high-purity metal In is pressed and broken into small blocks or powders, and 5N high-purity metal Se is also Crush into small pieces and put them into a quartz tube together, use a vacuum unit to evacuate the quartz tube to a vacuum of 10-3 Torr, and then seal the quartz tube; put the sealed tube filled with raw materials into a high-temperature box furnace for heating, and the double-temperature zone is dense. The tube synthesis method is that the sealed tube is kept at an atmospheric pressure, one end of the sealed tube is in the high temperature zone of the heating furnace, the temperature in the tube reaches 900-1000°C, and the other end is kept at 120-200°C in the water-cooled low-temperature zone, and the reaction in the tube is controlled. The In2Se3 compound was synthesized from In and Se within 4 hours; after the reaction in the tube was completed, the quartz tube was cut open, the In2Se3 pieces were poured out, and then vacuum-packed in a plastic bag with a vacuum degree of 10-1 Torr, and put into the finished product warehouse. The liquid phase synthesis process of the diindium triselenide double temperature zone vacuum tight tube of the invention is simple and safe in production.
Owner:江西科泰新材料有限公司

Preparation method of iron and nitrogen doped carbon nanoparticle photocatalyst

The invention relates to a preparation method of a chemical nanomaterial catalyst, and especially relates to a preparation method of an iron and nitrogen doped carbon nanoparticle photocatalyst. The method comprises the following steps: mixing materials: weighing 1.0g of a carbon source substance and 1.0g of a substance rich in amino groups, carboxyl groups and hydroxy groups, mixing the above substances in a 250mL beaker, adding 0.1g of iron trichloride, and adding a small amount of distilled water to dissolve above substances in order to obtain a purple solution; generating iron and nitrogen doped carbon nanoparticles: placing the solution in a constant temperature drying box, and heating at 210DEG C for 2h; and naturally cooling to obtain a brown-yellow foam solid in the beaker, wherein the solid is the iron and nitrogen doped carbon nanoparticles. The iron and nitrogen doped carbon nanoparticle solid is synthesized through direct co-heating with the carbon source substance and the substance rich in amino groups, carboxyl groups and hydroxy groups as precursors and iron trichloride as an iron source, so the method has the advantages of wide material sources, few synthesis steps, fast synthesis speed, no need of large scale devices, less investment, realization of macro production, and suitableness for industrial requirements.
Owner:SHENYANG UNIV
Who we serve
  • R&D Engineer
  • R&D Manager
  • IP Professional
Why Eureka
  • Industry Leading Data Capabilities
  • Powerful AI technology
  • Patent DNA Extraction
Social media
Try Eureka
PatSnap group products