On-line fixed carbon system and on-line fixed carbon evaluation method for movable bed device catalyst, and movable bed device

A catalyst and moving bed technology, applied in chemical instruments and methods, measuring devices, chemical analysis by combustion, etc., can solve the problems of low automation and efficiency, inability to monitor performance in real time, asynchronous catalyst analysis and production, etc.

Active Publication Date: 2018-11-30
SINOPEC LUOYANG TECH CO LTD +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0003] The establishment of an online monitoring and analysis system for various process materials in the refining and chemical process is an important part of building a smart factory. For the gas-liquid raw materials and products in the refining process, real-time online detection can be used to complete the monitoring of their physical properties and quality. The solid catalyst used in the refinery lacks an on-line detection method. There are problems such as the need to manually sample and analyze the catalyst regularly, the degree of automation and efficiency is low, and the analysis of the catalyst is not synchronized with the production. As a result, it is impossible to monitor its performance in all aspects in real time.

Method used

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  • On-line fixed carbon system and on-line fixed carbon evaluation method for movable bed device catalyst, and movable bed device

Examples

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Comparison scheme
Effect test

no. 1 example

[0047] Please refer to attached figure 1 , the present embodiment provides an online carbon determination system 10 for the catalyst of the moving bed device 200, which includes:

[0048] The first catalyst delivery pipe 101, the catalyst quantitative device 103, the second catalyst delivery pipe 105, the coke measurement reactor 107, the coke flue gas delivery pipe 120, the flue gas analyzer 121, the catalyst discharge pipe 110, and the third catalyst delivery Pipe 109, gas delivery pipe 111, material level gauge and flue gas discharge pipe 122. The online carbon determination system 10 can detect the amount of carbon deposition of the catalyst in the moving bed device 200 online and in real time, so as to determine the activity state of the catalyst in the moving bed device 200 .

[0049] Further, the discharge end of the first catalyst delivery pipe 101 is connected with the catalyst quantitative device 103, and the feed end of the first catalyst delivery pipe 101 is used ...

no. 2 example

[0067] This embodiment provides a moving bed device 200, which includes the online carbon determination system 10 provided in the first embodiment, please refer to the attached figure 1 , figure 1 The arrows in are the flow direction of the catalyst or the flow direction of the flue gas.

[0068] Specifically, the mobile device includes a reactor 201 and a regenerator 203 , and in this embodiment, a catalyst external circulation pipe 210 is provided between the reactor 201 and the regenerator 203 . The feed end of the catalyst external circulation pipe 210 is connected to the reactor 201 , and the discharge end of the catalyst external circulation pipe 210 is connected to the regenerator 203 . A small amount of catalyst is taken out from the reactor 201, and is continuously and stably transported to the regenerator 203 through the catalyst external circulation pipe 210 when not analyzing and sampling. The catalyst external circulation pipe 210 establishes a small circulation ...

no. 3 example

[0073] This embodiment provides a method for using the moving bed device 200 provided in the second embodiment to perform online carbon determination evaluation, and the specific steps are as follows:

[0074] System preparation:

[0075] Open the data processing terminal 123, preheat the flue gas analyzer 121 so that the flue gas analyzer 121 enters and maintains the ready state; open the nitrogen gas flow meter on the nitrogen gas delivery pipe 113 in the gas delivery pipe 111, and purge the reaction test system;

[0076] Catalyst collection and filling:

[0077] The catalyst is delivered intermittently or regularly from the catalyst external circulation pipe 210 of the moving bed device 200 through the first catalyst delivery pipe 101 to the catalyst quantitative device 103 for quantification. The last 3kg of catalyst enters into the coke measurement reactor 107 through the second catalyst delivery pipe 105, and carries out coke regeneration;

[0078] Scorch measurement r...

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Abstract

The invention relates to the technical field of petrochemical engineering development, and provides an on-line fixed carbon system for a movable bed device catalyst. The fixed carbon system comprisesa first catalyst conveying pipe, a catalyst quantification device, a second catalyst conveying pipe, a scorching measuring reactor, a scorching flue gas conveying pipe and a flue gas analyzer. The fixed carbon system can measure the amount of carbon deposit of the catalyst in real time under the condition of uninterrupted work of a movable bed device, improves the analysis efficiency of catalyst fixed carbon, and is fast, convenient and high in practicability. The embodiment of the invention also provides the movable bed device, wherein the movable bed device includes the on-line fixed carbonsystem, can understand the amount of carbon deposit of the catalyst in real time so as to judge the active state of the catalyst and improves the working efficiency of the movable bed device. In addition, the embodiment of the invention also provides the on-line fixed carbon evaluation method for the mobile bed device catalyst, wherein the method can quickly and real-timely monitor the state of the carbon deposit of the catalyst.

Description

technical field [0001] The invention relates to the technical field of petrochemical engineering development, in particular to an online carbon determination system for a catalyst in a moving bed device, an online carbon determination evaluation method thereof, and a moving bed device. Background technique [0002] The moving bed reactor is a reactor used to realize the gas-solid phase reaction process or liquid-solid phase reaction process. It is equipped with a catalyst circulation and regeneration system. The catalyst circulates between the reactor and the regenerator. After the reaction, the carbon-containing The catalyst is continuously regenerated in the regenerator and then sent back to the reactor for reaction. The catalyst in the moving bed reactor can be continuously regenerated, so the activity of the catalyst can be fully maintained and the severity of the reaction can be increased. Continuous regeneration moving bed is widely used in continuous reforming, movin...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B01J8/08B01J8/00G01N31/12G01N33/00
CPCB01J8/0015B01J8/008B01J8/08B01J8/082G01N31/12G01N33/0031G01N33/004
Inventor 李欣李治李静静沈方侠刘林娇韩海波刘丹禾郝代军
Owner SINOPEC LUOYANG TECH CO LTD
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