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Multi-pass process integration device

An integrated device and reactor technology, applied in the field of chemical transfer process equipment, can solve the problems of chemical reaction process reaction equipment danger, difficult heat transfer and mass transfer process control, temperature field and concentration field out of control, etc., to achieve convenient separation and Collect, meet multiphase flow mixing and reaction, avoid switching effect

Active Publication Date: 2020-12-25
ANHUI SCI & TECH UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

If the stirring cannot adjust the heat transfer or mass transfer in time, it will lead to the loss of control of the temperature field and concentration field in the system, which is a serious danger to the chemical reaction process and reaction equipment.
Hypergravity equipment and impinging flow equipment are ideal reaction equipment that can achieve rapid mixing, but their disadvantages are that the material residence time is short, which is suitable for rapid mixing and reaction processes
However, due to the dissipation and loss of ultrasonic waves and microwaves in the medium, it is difficult for ultrasonic waves and microwaves to effectively control the heat transfer and mass transfer processes inside large-volume reaction equipment. In industry, they are only used as a means of auxiliary mixing and heating. There are great limitations in the application of technology
For complex mixing processes or chemical reaction processes, the mixing requirements of different reaction stages are also different, and a single mixing method is difficult to meet, so it is necessary to increase the number of corresponding equipment, resulting in a longer process flow and increased energy consumption

Method used

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Experimental program
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Embodiment 2

[0044] Embodiment 2: as Figure 1-2, on the basis of Example 1, wherein the filler rotor is located at the top of the reactor, the stirring mechanism is located at the middle of the reactor, the ultrasonic-microwave emitting device is located at the bottom of the reactor, and several of them are driven by the same driving source; wherein the filler rotor is divided into It is a plurality of layers of rotating mechanisms, and several layers of rotating mechanisms are composed of several layers of concentric circles 22. The inner wall and outer wall of the ring are in a mesh structure, and from the outer ring to the inner ring, the meshes of the inner wall and the outer wall are constantly increasing. The top and bottom of the rings are plate-shaped structures, wherein the top and bottom edges of the rings are provided with rings 23, adjacent rings are connected by springs 24, and the two ends of the springs are connected to the rings.

[0045] The inner wall and the outer wall ...

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Abstract

The invention discloses a multi-transfer process integration device, and relates to the field of ultrasonic technology application equipment. The device mainly comprises a kettle body, wherein the upper end of the kettle body is provided with a feed inlet and the lower end is provided with a discharge outlet; the inside of the kettle body is mainly divided into an upper part and a lower part, andthe upper part mainly comprises a shaft arranged in the center of the upper end of the kettle body, a rotor arranged at the lower end of the shaft; the rotor is positioned in the kettle body; a trumpet-shaped collecting hopper is arranged on the inner wall of the kettle body; the collecting hopper has a small opening facing downwards; the lower part inside the kettle body mainly comprises a stirring main shaft which is connected and passes through the center of the bottom of the kettle body; a regular square ultrasonic transmitter is arranged in the center of the inner bottom of the kettle body; a stirring blade is arranged on the connecting stirring main shaft; and a connecting rod is arranged on the inner wall of the lower part in the kettle body and is connected with a connecting cylinder. The multi-transfer process integration device provided by the invention has a simple structure, is reasonably designed, and utilizes liquid for mixing and stirring for three times in the kettle, so that the liquid can be fully stirred, and the effect is obvious.

Description

Technical field: [0001] The invention relates to the field of chemical transfer process equipment, in particular to an integrated device with multiple mixing and heat transfer methods, including stirring mixing, ultrasonic mixing, impinging flow mixing, supergravity mixing, microwave heating, partition heat exchange and direct heat exchange hot. Background technique: [0002] Traditional stirring reaction equipment is a device widely used in mixing and chemical reactions in industry. Most of them operate intermittently and can be applied to momentum transfer, heat transfer and mass transfer processes. Stirred reaction equipment is greatly affected by the volume of the equipment. The interphase mass transfer and heat transfer process inside the reaction equipment is difficult to achieve the desired effect in a very short time, especially the chemical reaction process controlled by microscopic mixing and strong absorption and exotherm. The chemical reaction process is particu...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): B01J19/10
CPCB01J19/10
Inventor 郭雨黎少君冯纪章石国亮陈君华陈俊明
Owner ANHUI SCI & TECH UNIV