A kind of magnetic material adhesive and processing method thereof
A technology of magnetic materials and processing methods, applied in the directions of adhesives, non-polymer adhesive additives, adhesive additives, etc., can solve the problems of residual edge imprinting, etc., so as to save the mechanical grinding process, reduce the failure rate, and increase labor. The effect of efficiency
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Embodiment 1
[0015] A magnetic material adhesive, made of the following components in parts by weight: 96.0% ethyl α-cyanoacrylate, 2.9% diallyl phthalate, 0.03% phthalic anhydride, and 0.07% benzylsulfonic acid , Triethyl Citrate 1%.
[0016] The processing method of above-mentioned magnetic material adhesive comprises the following steps:
[0017] (1) Preparation of matrix glue auxiliary materials: In a 500L glass-lined reactor, add 348 kg of diallyl phthalate, start stirring, add 3.6 kg of phthalic anhydride and 8.4 kg of benzylsulfonic acid under continuous stirring conditions, mix The interlayer of the kettle is heated by steam, the temperature is controlled at 50-60°C, and stirred for 2-3 hours. The material in the kettle reaches a uniform and transparent fully dissolved state. Preparation and use;
[0018] (2) Preparation of matrix glue: In a 2000L enamel glass reaction kettle, add 1940kg of α-cyanoacrylate ethyl ester, under normal temperature conditions, under the condition of c...
Embodiment 2
[0021] A magnetic material adhesive, a magnetic material adhesive, is made of the following components in parts by weight: 95% ethyl α-cyanoacrylate, 2.9% diallyl phthalate, 0.03% phthalic anhydride, benzene Methanesulfonic acid 0.07%, triethyl citrate 2%.
[0022] The processing method of above-mentioned magnetic material adhesive comprises the following steps:
[0023] (1) Preparation of base glue auxiliary materials: In a 500L glass-lined reactor, add 348 kg of diallyl phthalate, start stirring, add 3.6 kg of phthalic anhydride and 8.4 kg of benzylsulfonic acid under continuous stirring, The interlayer of the mixing kettle is heated by steam, the temperature is controlled at 50-60°C, and stirred for 2-3 hours. The material in the kettle reaches a uniform and transparent fully dissolved state. Glue preparation and use;
[0024] (2) Preparation of matrix glue: In a 2000L enamel glass reaction kettle, add 1940kg of α-cyanoacrylate ethyl ester, under normal temperature condit...
Embodiment 3
[0027] A magnetic material adhesive, a magnetic material adhesive, is made of the following components in parts by weight: 94.0% ethyl α-cyanoacrylate, 2.9% diallyl phthalate, 0.03% phthalic anhydride, benzene Methanesulfonic acid 0.07%, triethyl citrate 3%.
[0028] The processing method of above-mentioned magnetic material adhesive comprises the following steps:
[0029] (1) Preparation of base glue auxiliary materials: In a 500L glass-lined reactor, add 348 kg of diallyl phthalate, start stirring, add 3.6 kg of phthalic anhydride and 8.4 kg of benzylsulfonic acid under continuous stirring, The interlayer of the mixing kettle is heated by steam, the temperature is controlled at 50-60°C, and stirred for 2-3 hours. The material in the kettle reaches a uniform and transparent fully dissolved state. Glue preparation and use;
[0030] (2) Preparation of matrix glue: In a 2000L enamel glass reaction kettle, add 1940kg of α-cyanoacrylate ethyl ester, under normal temperature cond...
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