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Method for preparing phellinus igniarius extract through micromolecule water and application

An extraction method and technology of small molecule water, which is applied in the field of preparing Phellinus Phellinus extract with small molecule water, can solve the problems of low content of active ingredients in the extract and low cream yield, and improve the utilization rate of Phellinus Phellinus and high cream yield , promote the effect of improving

Pending Publication Date: 2019-07-23
安徽省森湶谷药业股份有限公司 +1
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Therefore, the use of methods to improve the utilization of the active ingredients of Phellinus is the focus of current research. At present, the extraction methods of Phellinus include hot water extraction, decompression extraction, and ultrasonic extraction. Through experimental comparison, it is found that the compound extract of Phellinus The cream yield is low, and the content of active ingredients in the extract is low

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] The present embodiment provides a method for extracting Phellinus Phellinus, and the specific steps are as follows:

[0030] (1) select three-year-old Phellinus Phellinus with good quality as raw material;

[0031] (2) Use sodium dihydrogen phosphate-disodium hydrogen phosphate to adjust the pH of small molecule water to 7.5, wherein the concentration of sodium dihydrogen phosphate solution is 50mmol / l, the concentration of disodium hydrogen phosphate solution is 50mmol / l, dihydrogen phosphate Sodium solution 39ml, disodium hydrogen phosphate solution 61ml, the Phellinus coarse powder is crushed through a 50 mesh sieve, and the small molecule water, C1 enzyme, Cx enzyme, β-glucosidase and Phellinus powder, Phellinus regia powder are added successively in the container with a pH of 7.5. The mass ratio of yellow powder, C1 enzyme, Cx enzyme and β-glucosidase to small molecule water is 1: 0.1: 0.1: 0.1: 10, after mixing, use a homogenizer to homogeneously stir and mix, and...

Embodiment 2

[0038] The present embodiment provides a method for extracting Phellinus Phellinus, and the specific steps are as follows:

[0039] (1) select three-year-old Phellinus Phellinus with good quality as raw material;

[0040] (2) Regulating the pH of small molecule water with sodium dihydrogen phosphate disodium hydrogen phosphate is 7.0, wherein the concentration of sodium dihydrogen phosphate solution is 50mmol / l, the concentration of disodium hydrogen phosphate solution is 50mmol / l, sodium dihydrogen phosphate Solution 42ml, disodium hydrogen phosphate solution 59ml, pulverize Phellinus coarse powder through a 55 mesh sieve, add small molecule water with pH 7.0, C1 enzyme, Cx enzyme, β-glucosidase and Phellinus powder, Phellinus powder into the container successively , C1 enzyme, Cx enzyme and beta glucosidase and the mass ratio of small molecule water are 1: 1.0: 1.0: 1.0: 20, after mixing, stir and mix with homogenizer, the rotating speed of homogenizer is 10000r / min, Stir f...

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PUM

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Abstract

The invention discloses a method for preparing a phellinus igniarius extract through micromolecule water and an application. The method comprises the following steps of crushing phellinus igniarius, performing screening to obtain phellinus igniarius powder, sequentially adding the micromolecule water, enzymes and the phellinus igniarius powder to a container, and performing homogenizing, stirringand mixing so as to obtain mixed liquor; placing the mixed liquor in supercritical water reaction kettle, introducing reaction products into a condenser for condensing, and performing pressure filtration on the reaction products in a collector so as to obtain filtrate and filter residues; mixing the filter residues with the micromolecule water, then performing bifrequency ultrasonic extraction, filtering the extracted blending liquor by a centrifugal method so as to obtain filtrate and filter residues; mixing the filter residues with the micromolecule water, performing soxhlet extraction, andthen performing solid-liquid separation so as to obtain filter residues and filtrate; and mixing the separated filtrate, performing concentration on the mixed filtrate, and performing vacuum drying soas to obtain the phellinus igniarius composite extract. The phellinus igniarius composite extract is high in cream yield rate, the purity of effective components in the extract is high, and the utilization rate of the phellinus igniarius is effectively increased.

Description

technical field [0001] The invention belongs to the field of plant extraction, and in particular relates to a method and application for preparing Phellinus phellidis extract with small molecule water. Background technique [0002] Phellinus is a large perennial rare medicinal fungus. According to ancient medical records, Phellinus has "slightly bitter, cold, and non-toxic" properties. The main active ingredients of Phellinus Phellinus are polysaccharides, flavonoids, total phenols, ergosterol and other substances, which can be used as raw materials for tea, health care products and medicines. [0003] Phellinus Phellinus is difficult to plant and has a long growth cycle. The growth of high-quality Phellinus Phellinus requires a lot of manpower, material resources, and financial resources. Therefore, the use of methods to improve the utilization of the active ingredients of Phellinus is the focus of current research. At present, the extraction methods of Phellinus include h...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): A61K36/07
CPCA61K36/07A61K2236/19A61K2236/331A61K2236/37
Inventor 李宁陈刚孙贺春马良锯何露露胡娅张静刘幸樊家良
Owner 安徽省森湶谷药业股份有限公司
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