A kind of aqueous ethylene bis stearic acid amide emulsion and preparation method thereof

A technology of ethylene bis-stearic acid amide and emulsion, which is applied in directions such as inks, coatings, household appliances, etc., can solve the problems of easy precipitation, high production cost, flocculation layering and the like, so as to simplify the production process and save the production cost. , the effect of strong dispersing ability

Active Publication Date: 2021-08-31
广州正浩新材料科技有限公司
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

Due to the lack of special emulsifiers for ethylene bis stearic acid amide, even if the existing water-based ethylene bis stearic acid amide emulsions are added with emulsifiers, dispersants and anti-sedimentation agents, the dispersion effect is still poor, easy to precipitate, and long-term Flocculation and stratification will occur after time is left
In addition, the existing method requires high-speed stirring and grinding under heating conditions in the process of preparing water-based ethylene bis-stearic acid amide emulsion, the production process is complicated, and the production cost is high.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment 1

[0029] The preparation of embodiment 1 aqueous ethylene bis stearic acid amide emulsion

[0030] Composition in parts by weight of raw materials: 35 parts of ethylene bis stearic acid amide; 8 parts of emulsifier A; 2 parts of emulsifier B; 1 part of defoamer; 0.5 parts of preservative; 65 parts of deionized water.

[0031] The defoamer is polydimethylsiloxane; the preservative is methyl p-hydroxybenzoate. Described emulsifier B selects sorbitan fatty acid ester for use.

[0032] Described emulsifier A is prepared by the following method:

[0033] (1) Get cottonseed oil and dissolve it in ethylene glycol, then add sodium hydroxide, carry out heating and reflux reaction for 5h, and separate the product to obtain conjugated cottonseed oil; the volumetric dosage of described ethylene glycol is 8 times of the volumetric dosage of cottonseed oil; The weight consumption of described sodium hydroxide is 25% of cottonseed oil weight.

[0034] (2) Add conjugated cottonseed oil and m...

Embodiment 2

[0038] The preparation of embodiment 2 aqueous ethylene bis stearic acid amide emulsion

[0039] Composition in parts by weight of raw materials: 30 parts of ethylene bis stearic acid amide; 5 parts of emulsifier A; 1 part of emulsifier B; 1 part of defoamer; 0.5 parts of preservative; 70 parts of deionized water.

[0040] The defoamer is polydimethylsiloxane; the preservative is methyl p-hydroxybenzoate. Described emulsifier B selects sorbitan fatty acid ester for use.

[0041] Described emulsifier A is prepared by the following method:

[0042] (1) Get cottonseed oil and dissolve it in ethylene glycol, then add sodium hydroxide, carry out heating and reflux reaction for 6h, and separate the product to obtain conjugated cottonseed oil; the volumetric dosage of described ethylene glycol is 5 times of the volumetric dosage of cottonseed oil; The weight consumption of described sodium hydroxide is 30% of cottonseed oil weight.

[0043] (2) Add conjugated cottonseed oil and ma...

Embodiment 3

[0047] The preparation of embodiment 3 aqueous ethylene bis stearic acid amide emulsion

[0048] Composition of raw materials in parts by weight: 40 parts of ethylene bis stearic acid amide; 10 parts of emulsifier A; 3 parts of emulsifier B; 1 part of defoamer; 0.5 parts of preservative; 60 parts of deionized water.

[0049] The defoamer is polydimethylsiloxane; the preservative is methyl p-hydroxybenzoate. Described emulsifier B selects sorbitan fatty acid ester for use.

[0050] Described emulsifier A is prepared by the following method:

[0051] (1) Get cottonseed oil and dissolve it in ethylene glycol, then add sodium hydroxide, carry out heating and reflux reaction for 4h, and separate the product to obtain conjugated cottonseed oil; the volumetric dosage of described ethylene glycol is 10 times of the volumetric dosage of cottonseed oil; The weight consumption of described sodium hydroxide is 20% of cottonseed oil weight.

[0052] (2) Add conjugated cottonseed oil and m...

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Abstract

The invention relates to the technical field of preparation of ethylene bis-stearic acid amide emulsion, and specifically discloses a water-based ethylene bis-stearic acid amide emulsion and a preparation method thereof. The water-based ethylene bis-stearic acid amide emulsion comprises the following components in parts by weight: 30-40 parts of ethylene bis-stearic acid amide; 5-10 parts of emulsifier A; 1-3 parts of emulsifier B; 1-2 parts of foaming agent; 0.1-1 part of preservative; 60-70 parts of deionized water. The water-based ethylene bis-stearic acid amide emulsion has a simple production process, good dispersion effect, and can be stored for a long time.

Description

technical field [0001] The invention relates to the technical field of preparation of ethylene bis-stearic acid amide emulsion, in particular to a water-based ethylene bis-stearic acid amide emulsion and a preparation method thereof. Background technique [0002] Ethylene bis-stearamide, also known as vinyl bis-stearamide, is a hard and brittle white high-melting point wax. Its industrial products are small yellowish particles. It is non-toxic, has no side effects on the human body, and is insoluble at room temperature. For most solvents, it is often used as plastic lubricants and additives for paints and inks. [0003] Since ethylene bis stearic acid amide is insoluble in water, it is usually necessary to add emulsifiers, dispersants, solubilizers and anti-settling agents in the process of preparing water-based ethylene bis stearic acid amide emulsions to achieve dispersion and anti-settling effects. Due to the lack of special emulsifiers for ethylene bis stearic acid amid...

Claims

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Application Information

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Patent Type & Authority Patents(China)
IPC IPC(8): C08L91/00C08L83/04C08K5/20C08K5/134C08K5/1535C09D7/63C09D7/65C09D11/03
CPCC08L91/00C09D11/03C09D7/63C09D7/65C08L83/04C08K5/20C08K5/1345C08K5/1535
Inventor 李英
Owner 广州正浩新材料科技有限公司
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