Modification method for improving shape memory performance of gutta-percha rubber

A technology of eucommia glue and modification, applied in the field of material modification, can solve the problems of low utilization rate of eucommia glue, mismatched temperature range of asphalt pavement, single modification method, etc., so as to reduce maintenance costs and resource consumption, and speed up national The effect of economic development and enrichment of modification methods

Active Publication Date: 2019-11-12
NANJING FORESTRY UNIV
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

[0010] The purpose of the present invention is to provide a modification method for improving the shape memory performance of eucommia gum, which solves the problem that the existing modification method of eucommia gum is single, the shape memory performance after modification is poor, and the crystallization temperature does not match the temperature range of the asphalt pavement, which leads to the utilization of eucommia gum. It is difficult to improve the shape memory performance and self-healing function of asphalt pavement, reduce the cracks of asphalt pavement or reduce the width of cracks when used in modified asphalt
[0012] In order to solve the current modification method of eucommia gum, the shape memory performance after modification is poor, and the crystallization temperature does not match the temperature range of asphalt pavement, resulting in low utilization rate of eucommia gum, and it is difficult to improve the shape memory performance of asphalt pavement and Self-healing features, problems reducing asphalt pavement cracks or reducing crack width

Method used

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Experimental program
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Effect test

Embodiment Construction

[0016] The invention provides a modification method for improving the shape memory performance of eucommia gum, and the specific implementation steps are as follows:

[0017] (1) Start the Brabender plasticizing internal mixer, and preheat it for 2 minutes, preheat the temperature of the feeding port and the mixing head to 70°C, and set the roller shaft speed to 50r / min;

[0018] (2) Add a certain amount of bulk Eucommia gum in batches, after the Eucommia gum is heated and softened and mixed evenly, add a certain amount of zinc oxide powder, stearic acid and anti-aging agent 4010NA, and knead at 70°C for 7 minutes;

[0019] (3) Add a certain amount of N-cyclohexyl-2-benzothiazole sulfenamide and different amounts of dibenzoyl peroxide into the Brabender plasticizing internal mixer, and set the roller shaft speed to 80r / min, mixing for 15min;

[0020] (4) Peel off the eucommia gum after the full reaction, place it on a molding machine, set the temperature at 160°C, the pressu...

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Abstract

The invention provides a modification method for improving the shape memory performance of gutta-percha rubber and belongs to the technical field of material modification. Through the modification method, the problems that an existing gutta-percha rubber modification method is single, the shape memory performance is poor, the crystallization temperature is not matched with the asphalt pavement using temperature range and the gutta-percha rubber is low in utilization rate and can hardly improve the shape memory performance and the self-repairing function of an asphalt pavement when used for modifying asphalt and reduce asphalt pavement cracks or the crack width are solved. The modification method comprises the steps of firstly, preparing the modified gutta-percha rubber with the shape memory performance; secondly, conducting mold pressing on the gutta-percha rubber subjected to sufficient reaction and giving the shape memory performance to the gutta-percha rubber; and finally, carryingout a performance study through related instruments to determine that the modified gutta-percha rubber has the optimum shape memory performance. Through the modified gutta-percha rubber prepared through the method, the asphalt can be modified, and the asphalt pavement has the shape memory performance. Meanwhile, the gutta-percha rubber is modified, the modification manner of the gutta-percha rubber is enriched, and the utilization rate of the gutta-percha rubber is improved.

Description

technical field [0001] The invention relates to a modification method for improving the shape memory performance of eucommia gum, belonging to the technical field of material modification. Background technique [0002] In recent years, great breakthroughs have been made in the research on the application of eucommia gum. Since its molecular chain structure has three characteristics of double bond vulcanization, orderliness, and chain flexibility, it has great potential for development. Eucommia gum is divided into natural Eucommia gum (EUG) and synthetic Eucommia gum (TPI). EUG is mainly derived from the Eucommia tree, and China has more than 95% of the Eucommia tree resources in the world. Domestic TPI mainly comes from individual new material companies, which have 10,000-ton-level trans-isoprene rubber industrial production equipment, which can provide a large number of new high-quality raw materials for various researches. In the 1980s, Eucommia gum elastomer was prepare...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): B29C69/00C08L7/00C08K13/02C08K3/22C08K5/09C08K5/18C08K5/47C08K5/14
CPCB29C69/00C08K3/22C08K5/09C08K5/14C08K5/18C08K5/47C08K13/02C08K2003/2296C08L2201/12C08L7/00
Inventor 许涛李宁许俊杰王宏畅
Owner NANJING FORESTRY UNIV
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