Method to improve visibility of contents, vinyl chloride-based resin composition, stabilizer, vinyl chloride-based resin molded body, medical material, and sterilization processing method
A technology for vinyl chloride resins and medical materials, applied in the field of medical materials for the visibility of contents, can solve problems such as decline, inability to obtain results, and difficulty in suppressing transparency.
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[0198] Examples are given below to illustrate the present invention in more detail, but the present invention is not limited by these examples. In addition, the abbreviated symbols and the measurement of each characteristic of the compound in an Example and an application example are as follows.
[0199] 〔Measurement and evaluation method〕
[0200] (1) The carbon number of saturated fatty alcohol and the ratio of linear saturated fatty alcohol
[0201] Among the 4-cyclohexene-1,2-dicarboxylic acid diesters or 4,5-epoxy-1,2-cyclohexanedicarboxylic acid diesters used in Examples and Comparative Examples of the present invention, for The carbon number of the saturated fatty alcohol that determines the residue in the general formula (1) or (2) and the ratio of the straight-chain saturated fatty alcohol are measured by gas chromatography (hereinafter abbreviated as GC) to the raw material alcohol used for its production. As a result of the composition in these compounds, the rati...
manufacture example 1
[0230] In a 1L four-neck flask equipped with a thermometer, a decanter, a stirring blade, and a reflux cooling pipe, 182.6 g (1.2 moles, manufactured by Shin Nippon Chemical Co., Ltd.) of 4-cyclohexene-1,2-dicarboxylic anhydride was added. Rikacid TH), 374 g (2.9 mol) of 2-ethylhexyl alcohol, and 0.24 g of tetraisopropyl titanate as an esterification catalyst were used, and the reaction temperature was set at 200° C. to carry out the esterification reaction. The reaction was performed until the acid value of the reaction solution reached 0.5 mgKOH / g while refluxing the alcohol under reduced pressure and removing generated water to the outside of the system. After the reaction, the unreacted alcohol was distilled out of the system under reduced pressure, and then neutralized, washed with water, and dehydrated according to a common method to obtain the target stabilizer compound of the present invention, 4-cyclohexene- 369 g of 1, 2- dicarboxylic-acid diester (henceforth "compou...
manufacture example 2
[0233] As a substitute for 374 g (2.9 mol) of 2-ethylhexyl alcohol, an aliphatic saturated alcohol containing 88.5 mol% of a straight-chain saturated fatty alcohol with 9 carbon atoms and 11.1 mol% of a branched-chain saturated fatty alcohol with 9 carbon atoms was added. Alcohol (manufactured by Shell Chemicals, product name: Linevol 9) 416g (2.9 moles), except that, it was carried out in the same manner as in Production Example 1, and 4-cyclohexene-1, which was the stabilizer compound of the present invention, was obtained. 449 g of 2-dicarboxylic acid diester (henceforth "compound 2").
[0234] The obtained compound 2 had an ester value: 260 mgKOH / g, an acid value: 0.04 mgKOH / g, and a chroma: 10.
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