Honeycomb ceramic for adsorbing and inactivating viruses, and application thereof
A honeycomb ceramic and virus technology, applied in applications, ceramic products, adsorbed water/sewage treatment, etc., can solve the problems of easy shedding of active components, low activity, and poor sterilization effect.
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[0042] The preparation of catalytic material of the present invention comprises the steps:
[0043] 1. Preparation of powdery core-shell structured hierarchical porous materials
[0044] (1) Preparation of nucleus: NH 4 ZSM-5 molecular sieve (SiO 2 / Al 2 o 3 =25, the specific surface area is 550m 2 / g, particle size 2.3μm, average pore size 0.54nm) mixed with 0.35mol / L NaOH solution at a volume ratio of 1:30, heated and stirred in a water bath at 75°C for 2 hours, filtered the mixed solution, and washed the solid until neutral , after drying at 120°C for 6 hours and calcining at 500°C for 2 hours, a hierarchical porous molecular sieve, which is the core of the catalytic material, was obtained. Measure its average mesopore diameter 24.3nm with the automatic physical adsorption instrument (US Micromeritics company, ASAP 2460) that can measure the distribution and pore volume of mesopore and micropore, the pore distribution is 3.2-48.7nm, and the average micropore diameter i...
Embodiment 1-4
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Embodiment 5-20
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[0068] 2. Adsorption and inactivation test for viruses
[0069] 1. Virus preparation:
[0070] Prepare TCID separately 50 COVID-19 virus liquid (75ng / ul) and TCID 50 The tool lentivirus (pLenti) virus liquid (100ng / ul) is used for the adsorption and inactivation test of new coronavirus and lentivirus by powder materials and honeycomb ceramics;
[0071] 2. Prepare 9 kinds of honeycomb ceramic small blocks, numbered HX-1-9, weigh 0.5g of each material, and 0.5g of honeycomb ceramic matrix of unloaded core-shell structure multi-level porous material, put them into sterile 1.5 ml EP tube, add 1.0mL TCID dropwise 50 The lentivirus (pLenti) virus liquid was reacted at room temperature for 30 minutes, and the mixture of the test substance and the virus liquid was shaken with a shaker at intervals of 5 minutes during this period to ensure the full effect of the material and the virus. At the same time, prepare a blank con...
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