Polyimide-based film and window cover film including the same
A polyimide-based film and polyimide technology, applied in the input/output process of data processing, identification devices, instruments, etc., can solve problems such as poor visibility, light diffuse reflection, eye fatigue, etc.
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[0067] An exemplary preparation step of the film of the present invention is generally carried out by the following steps: the polyimide-based resin solution is discharged onto a support (substrate) such as a stainless steel belt, glass, film, etc. through a die (Die) Coating steps, drying steps and stretching steps, if necessary, can be prepared by further drying steps after stretching, and can be prepared by changing and adjusting the above-mentioned conditions so as to have the desired physical properties of the present invention , but the method is not particularly limited.
[0068] As an example, when describing the coating step of providing the film of the present invention, the coating step is a step of coating a resin solution on a substrate through a casting die, and adjusting the shear rate generated when the resin solution passes through the die. The shear rate and the air gap (air gap) which is the distance from the die lip portion to the surface of the support can...
Embodiment 1
[0162] In a mixed solution of dichloromethane and pyridine, mix isophthaloyl chloride (IPC), terephthaloyl chloride (TPC) and 2,2′-bis(trifluoromethyl )-benzidine (TFMB), stirred at 25° C. for 2 hours in a reactor under nitrogen atmosphere. The solids content was 10% by weight. After the above reaction, the reactant was precipitated in water, filtered, and the solid was vacuum-dried at 50° C. for 6 hours or more to obtain an oligomer. The molecular weight (FormulaWeight, FW) of the oligomer was 11580 g / mol.
[0163] In a reactor, using N,N-dimethylacetamide (DMAc) as a solvent, 100 moles of the oligomer and 20 moles of 2,2′-bis(trifluoromethyl)-benzidine ( TFMB) and stir well. After confirming that solid raw material dissolves completely, with respect to described solid, fumed silica (surface area is 95m 2 / g, <1μm) was added to DMAc at a content of 1000ppm, dispersed and added by ultrasonic waves. 120 mol of cyclobutanetetracarboxylic dianhydride (CBDA) was added and sti...
Embodiment 2
[0168] It was prepared by the same method as in Example 1 except that the wind speed in the drying section was 10 m / s.
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