Separator and electrochemical device comprising same
An electrochemical and separator technology, applied in electrochemical generators, hybrid capacitor separators, circuits, etc., can solve the problem of high explosion risk of separators, and achieve the effect of high bonding strength and increasing Lamie strength
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Embodiment 1
[0105] P(VDF-TrFE-CTFE) (β-phase content: 0.98) and PVDF-CTFE as a binder polymer were added to an acetone solvent at a weight ratio of 50:50, and dissolved at 50°C for about 4 hours to Prepare the binder polymer solution. In this case, the ratio of solvent to solids (weight of slurry from which solvent was removed) in the binder polymer solution was 19:1.
[0106] Subsequently, the binder polymer solution was dip-coated on both surfaces of a 9 μm-thick polyethylene porous polymer substrate (porosity: 43%, air permeation time: 110 seconds, resistance 0.45Ω), and heated at 23°C and Dry at a relative humidity of 40% to fabricate separators with porous coatings.
Embodiment 2
[0108] P(VDF-TrFE-CTFE) (β-phase content: 0.98) and PVDF-CTFE as a binder polymer were added to an acetone solvent at a weight ratio of 50:50, and dissolved at 50°C for about 4 hours to Prepare the binder polymer solution. Subsequently, alumina (Al 2 o 3 ) (particle size: 500nm) and boehmite (AlOOH) (particle size: 250nm) were mixed at a weight ratio of 9:1, and added to the binder polymer solution so that the weight of the binder polymer and inorganic particles The ratio is 20:80. 2 parts by weight of a dispersant based on 100 parts by weight of the inorganic particles were added, and the inorganic particles were pulverized and dispersed for 12 hours using a ball milling method to prepare a porous coating layer forming slurry. In this case, the ratio of solvent to solid was controlled at 4:1.
[0109] The porous coating-forming slurry was dip-coated on both surfaces of a 9 μm-thick polyethylene porous polymer substrate (porosity: 43%, air permeation time: 110 seconds, res...
Embodiment 3 to Embodiment 4
[0111] Separators were produced in the same manner as in Example 2, except that the amounts of P(VDF-TrFE-CTFE) and PVDF-CTFE were adjusted as shown in Table 1.
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