Method for producing graphite base composite material for electromagnetic shield
A composite material and graphite-based technology, applied in the direction of magnetic/electric field shielding, electrical components, etc., can solve problems such as complex processes, achieve simple preparation processes, improve electromagnetic shielding performance, and overcome difficulties in uniform distribution to the graphite matrix.
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Embodiment 1
[0026] (1) expandable graphite and ferrocene crystal powder with a mass ratio of 1.25: 1 are uniformly mixed by mechanical physics;
[0027] (2) Put the mixture into an atmosphere at 1000°C, and the expandable graphite will expand rapidly to obtain expanded graphite worms with magnetic particles attached;
[0028] (3) Press the obtained expanded graphite worms into a disc with a diameter of 16 mm and a thickness of about 1 mm in a mold.
[0029] The microscopic morphology of the prepared expanded graphite worms attached with magnetic particles is as follows: figure 1 As shown, it can be seen that the magnetic particles have been uniformly mixed into the worms of expanded graphite; the microscopic morphology of the disc sample manufactured by this method is as follows figure 2 Shown; The hysteresis loop of the disc sample is tested with a vibrating magnetometer (VSM, Lake Shore 7307), and the results are as follows image 3 As shown, it can be seen from the figure that the s...
Embodiment 2
[0031] (1) expandable graphite and ferrocene crystal powder with a mass ratio of 5: 1 are uniformly mixed by mechanical physics;
[0032] (2) Put the mixture into an atmosphere at 700°C, and the expandable graphite will expand rapidly to obtain expanded graphite worms with magnetic particles attached;
[0033] (3) Press the obtained expanded graphite worms into a disc with a diameter of 16 mm and a thickness of about 1 mm in a mold.
[0034] The electrical conductivity of the sample was tested by the van der Pauw method in the four-point probe method, and its volume resistivity was 1.39×10 -3 Ω·cm.
Embodiment 3
[0036] (1) expandable graphite and nickel hydroxide powder with a mass ratio of 2.5: 1 are mixed uniformly by mechanical physics;
[0037] (2) Put the mixture into an atmosphere at 1100°C, and the expandable graphite will expand rapidly to obtain expanded graphite worms with magnetic particles attached;
[0038] (3) Press the obtained expanded graphite worms into a disc with a diameter of 16 mm and a thickness of about 1 mm in a mold.
[0039] The electrical conductivity of the sample was tested by the van der Pauw method in the four-point probe method, and its volume resistivity was 0.962×10 -3 Ω cm, electromagnetic shielding performance see Figure 6 .
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