Shape memory styrene copolymer
A memory polymer, styrene technology, used in eye implants, instruments, other household appliances, etc.
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Embodiment 1
[0039] A polymerization mixture was prepared by mixing vinyl neodecanoate (7%), divinylbenzene (1%), and styrene (90%) in any order to produce a clear solution. Benzoyl peroxide (2%) was then added to the resulting solution (all component % are by weight). Store the resulting solution in the refrigerator until use. To prepare the shape memory polymer (SMP), the reaction mixture prepared above was injected with a syringe into a mold prepared with two 14"x14" glass plates separated by a Viton spacer. The two glass plates are then clamped together along the edges with clamps. The Viton gasket also acts as a seal in the mold. The sample was then heated for 24 hours in an oven maintained at atmospheric pressure and a temperature of 75°C. After curing the sample for the specified time, remove it from the oven and immediately transfer it to a warm water bath. The temperature of the water used was about 60°C. The formed SMP sheet was demolded in the warm water by applying slight ...
Embodiment 2
[0042] A polymerization mixture was prepared by mixing vinyl neodecanoate (7%), divinylbenzene (1%), and styrene (60%) in any order to give a colorless solution. Polystyrene particles (30%) were then added to the resulting solution. The resulting mixture was then left at room temperature with occasional stirring until all the polystyrene particles were dissolved to give a clear viscous solution. Benzoyl peroxide (2%) was then added to the resulting solution (all component % are by weight). The resulting mixture was sonicated at room temperature for 15 minutes to give a clear solution. The resulting solution was refrigerated until use. To prepare the shape memory polymer (SMP), the reaction mixture prepared above was injected with a syringe into a mold prepared with two 14"x14" glass plates separated by a Viton spacer. The two glass pieces are then clamped together along the edges with clamps. The Viton gasket also acts as a seal in the mold. The sample was then heated for...
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