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Resin composition

A resin composition and a technology for the composition, applied in the field of resin compositions, can solve the problems of increased dielectric constant and low acid resistance, achieve improved acid resistance, good dispersibility, avoid poor heat resistance and increased dielectric constant. high effect

Inactive Publication Date: 2007-04-18
NISSHINBO IND INC
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  • Summary
  • Abstract
  • Description
  • Claims
  • Application Information

AI Technical Summary

Problems solved by technology

That is to say, although a high filling amount can be achieved by improving the dispersibility on the one hand, new problems such as low acid resistance and high dielectric constant of the molded products obtained will arise.

Method used

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Examples

Experimental program
Comparison scheme
Effect test

Embodiment

[0122] Hereinafter, the present invention will be specifically described by listing synthesis examples, examples, and comparative examples, but the present invention is not limited to the following examples.

[0123]

Synthetic example 1 2

[0124] [Synthesis Example 1] Synthesis of bis(trifluoromethanesulfonimide) salt of diethylmethyl(2-methoxyethyl)ammonium (hereinafter abbreviated as DEME·TFSI)

[0125] 100 ml of diethylamine (manufactured by Kanto Chemical Co., Ltd.) and 85 ml of 2-methoxyethyl chloride (manufactured by Kanto Chemical Co., Ltd.) were mixed, and the resulting mixed solution was placed in an autoclave and reacted at 100° C. for 24 Hour. At this time, the internal pressure is 0.127MPa (1.3kfg / cm 2 ). After 24 hours, 200 ml of an aqueous solution in which 56 g of potassium hydroxide (manufactured by Katayama Chemical Industry Co., Ltd.) was dissolved was added to the mixture of the precipitated crystal and the reaction solution, and the organic layer divided into two layers was separated with a splitting funnel. Further, 100 ml of dichloromethane (manufactured by Wako Pharmaceutical Industries, Ltd.) was added, and two extraction operations were performed.

[0126] The separated organic layers...

Synthetic example 2 2

[0131] [Synthesis Example 2] Diethylmethyl (2-methoxyethyl) ammonium tetrafluoroborate (hereinafter referred to as DEME·BF 4 )Synthesis

[0132] 15.0 g of 2-methoxyethyldiethylmethylammonium iodide synthesized in the same manner as in Synthesis Example 1 was dissolved in 100 ml of distilled water, and 6.37 g of silver oxide (Kanto Chemical Co., Ltd.) was added to the solution. production) and stirred for 3 hours. After the precipitate was removed by filtration under reduced pressure, 42% tetrafluoroboric acid (manufactured by Kanto Chemical Co., Ltd.) was added a little at a time with stirring to bring the pH of the reaction solution around 5 to 6. The reaction solution was freeze-dried, and then the water was fully distilled off with a vacuum pump to obtain 12.39 g of DEME·BF which was liquid at room temperature (25°C). 4 . This method is carried out several times to synthesize the desired amount.

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Abstract

Disclosed is a resin composition wherein dispersibility of a modifying agent such as an inorganic substance is improved. The acid resistance of this resin composition is not deteriorated even when a modifying agent is blended therein. Specifically, the resin composition includes a base material having a cyano group-containing organic layer and an organic resin. This resin composition is extremely excellent in acid resistance when compared with organic resins which use a base material having an organic layer not containing a cyano group.

Description

technical field [0001] The present invention relates to a resin composition, and more particularly, the present invention relates to a resin composition formed by compounding a substrate having a cyano group-containing organic layer on its surface. Background technique [0002] Conventionally, organic resins have been processed into films or other molded products and used for various purposes. [0003] In this case, in order to improve the performance of the molded product and make the molded product exhibit special functions, it is often necessary to add an inorganic substance as a modifier to the organic resin. A molded product formed of a composition obtained by adding a modifier to an organic resin has the advantage of combining the characteristic properties of the modifier and the organic substance, and thus has been used in a wide range of fields. [0004] However, when a modifier such as an inorganic substance is blended into a matrix resin, etc., if the dispersibili...

Claims

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Application Information

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Patent Type & Authority Applications(China)
IPC IPC(8): C08K9/04C08L101/00C08F292/00C08L51/10
CPCC08K9/04C08L101/00C08L51/10
Inventor 增田现桥场俊文早川和寿塚本奈巳
Owner NISSHINBO IND INC