Method for Producing a Latent Heat Storage Material and Dialkyl Ether as a Latent Heat Storage Material
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experiment 1
[0039]Dehydrating fatty alcohols to linear olefins 2474 g of NACOL® 16-99 (purity 99.5%, based on renewable raw materials) were mixed with 500 g of Al2O3 and 60 ml of xylene in a 6 l flask and heated at up to 295° C. at the water separator for 4.5 hours. In that, 180 ml of water were formed. The hexadecene formed was distilled in vacuum. The yield was a mixture of alpha- and internal olefins.
experiment 2
[0040]Hydrating linear olefins to linear paraffins 685 g of the hexadecene obtained in Experiment 1 were hydrated for 7 hours at 98° C. according to a known method over a heterogeneous Ni-containing catalyst at 20 bar H2 pressure and filtrated after cooling.
[0041]Fatty alcohols with chain lengths of C16 to C22 were used according to Experiments 1 and 2, and the following paraffins were obtained:
TABLE 2ParaffinHexadecaneOctadecaneEicosaneDocosanen-paraffin (main99.698.893.297.4component) [%]n-paraffin99.898.996.898.6(total) [%]iso-paraffin [%]0.20.11.81.2Onset [° C.]17.427.432.540.6Melting heat [J / g]245.6250.7247.2270.5
experiment 3
[0042]Experiments 1 and 2 were repeated, however, a synthetic fatty alcohol (hexadecanol) from the Ziegler process with a purity of 95.6% was used as the alcohol.
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