Method of producing patterned birefringent product and birefringent pattern building material
a technology of birefringent and product, which is applied in the direction of instruments, polarising elements, photomechanical equipment, etc., can solve the problems of insufficient design properties, insufficient thermal resistance, and inability to align high-molecular cholesteric liquid crystals at the same tim
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example 1
Production of Birefringent Pattern Building Material Showing Green Characteristic Reflection and Cholesteric Pattern Product
(Preparation of Coating Liquid for Dynamic Property Controlling Layer CU-1)
[0210]The composition below was prepared, filtered through a polypropylene filter having a pore size of 30 μm, and the filtrate was used as a coating liquid for forming a dynamic property controlling layer CU-1.
[0211]
Composition of Coating Liquid for Dynamic property controlling Layer(% by mass)Methyl methacrylate / 2-ethylhexyl acrylate / benzyl5.89methacrylate / methacrylic acid copolymer (copoly-merization ratio (molar ratio) = 55 / 30 / 10 / 5, mass-average molecular weight = 100,000, Tg: about 70° C.)Styrene / acrylic acid copolymer (copolymerization 13.74ratio (molar ratio) = 65 / 35, mass-averagemolecular weight = 10,000, Tg: about 100° C.)Dimethacrylate of Ethoxylated Bisphenol A9.20BPE-500 (trade name, manufactured by Shin-Nakamura Chemical Co., Ltd.)Fluorine series surfactant0.55Megafac F-780-...
example 2
Production of Birefringent Pattern Building Material Showing Blue Characteristic Reflection and Cholesteric Pattern Product
(Preparation of Coating Liquid for Optically Anisotropic Layer LC-2)
[0229]The composition below was prepared, filtered through a polypropylene filter having a pore size of 0.2 μm, and the filtrate was used as coating liquid for forming an optically anisotropic layer LC-2.
[0230]
Composition of Coating Liquid for Optically Anisotropic Layer(% by mass)Rod-like liquid crystal (LC-1-1)30.67Chiral Agent (Paliocolor LC756, trade name, 1.83manufactured by BASF Japan Ltd.)Horizontal aligning agent (LC-1-2)0.10Cationic photopolymerization initiator (CPI100-P, 0.67trade name, manufactured by San-Apro Ltd.)Polymerization control agent (IRGANOX 1076, trade name,0.07manufactured by Ciba Specialty Chemicals Corporation)Methyl ethyl ketone66.66
(Production of Cholesteric Pattern Building Material CPM-2)
[0231]Transferring material for producing cholesteric pattern, TR-2, was prepa...
example 3
Production of Birefringent Pattern Building Material Showing Red Characteristic Reflection and Cholesteric Pattern Product
(Preparation of Coating Liquid for Optically Anisotropic Layer LC-3)
[0233]The composition below was prepared, filtered through a polypropylene filter having a pore size of 0.2 μm, and the filtrate was used as coating liquid for forming an optically anisotropic layer LC-3.
[0234]
Composition of Coating Liquid for Optically AnisotropicLayer(% by mass)Rod-like liquid crystal (LC-1-1)31.13Chiral Agent (Paliocolor LC756, trade name, 1.37manufactured by BASF Japan Ltd.)Horizontal aligning agent (LC-1-2)0.10Cationic photopolymerization initiator (CPI100-P, 0.67trade name, manufactured by San-Apro Ltd.)Polymerization control agent (IRGANOX 1076, trade name,0.07manufactured by Ciba Specialty Chemicals Corporation)Methyl ethyl ketone66.66
(Production of Cholesteric Pattern Building Material CPM-3)
[0235]Transferring material for producing cholesteric pattern, TR-3, was prepare...
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